(3R,4R)-1-tert-butyl-4-carboxy-3-(2,4-difluoro-phenyl)pyrrolidinium chloride

Base Information

• Chemical Name: (3R,4R)-1-tert-butyl-4-carboxy-3-(2,4-difluoro-phenyl)pyrrolidinium chloride
• CAS No.: 1346012-72-3
• Molecular Formula: C₁₆H₂₁F₂NO₂*ClH
• Molecular Weight: 333.806

Synonyms:(3R,4R)-1-tert-butyl-4-carboxy-3-(2,4-difluoro-phenyl)pyrrolidinium chloride

Chemical Property of (3R,4R)-1-tert-butyl-4-carboxy-3-(2,4-difluoro-phenyl)pyrrolidinium chloride

Chemical Property:

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Technology Process of (3R,4R)-1-tert-butyl-4-carboxy-3-(2,4-difluoro-phenyl)pyrrolidinium chloride

There total 1 articles about (3R,4R)-1-tert-butyl-4-carboxy-3-(2,4-difluoro-phenyl)pyrrolidinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S) tert-butyl-4-(2-{1-[acetyl(isopropyl)amino]ethyl}-5-chloro-4-methylphenyl)piperazine-1-carboxylate (757245-90-2) → (3R,4R)-1-tert-butyl-4-carboxy-3-(2,4-difluoro-phenyl)pyrrolidinium chloride (1346012-72-3)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; dichloromethane; at 20 ℃; for 0.5h;

Reference yield:

(3R,4R)-1-tert-butyl-4-carboxy-3-(2,4-difluoro-phenyl)pyrrolidinium chloride (1346012-72-3) → N-{1S}-1-[2-(4-{[(3R,4R)-1-tert-butyl-3-(2,4-difluorophenyl)piperidine-4-yl]carbonyl}piperazine-1-yl)-4-chloro-5-methylphenyl]ethyl-N-isopropylacetamide

Guidance literature:

With 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU; In dichloromethane; at 20 ℃;

upstream raw materials:

(S) tert-butyl-4-(2-{1-[acetyl(isopropyl)amino]ethyl}-5-chloro-4-methylphenyl)piperazine-1-carboxylate

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