N-(1-methylheptanyl)-N-phenyl-2-(1,3-dioxan-2-yl)ethylsulfonamide

Base Information

Chemical Name:N-(1-methylheptanyl)-N-phenyl-2-(1,3-dioxan-2-yl)ethylsulfonamide
CAS No.:874979-47-2
Molecular Formula:C₂₀H₃₃NO₄S
Molecular Weight:383.552
Hs Code.:

Synonyms:N-(1-methylheptanyl)-N-phenyl-2-(1,3-dioxan-2-yl)ethylsulfonamide

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Chemical Property of N-(1-methylheptanyl)-N-phenyl-2-(1,3-dioxan-2-yl)ethylsulfonamide

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Technology Process of N-(1-methylheptanyl)-N-phenyl-2-(1,3-dioxan-2-yl)ethylsulfonamide

There total 3 articles about N-(1-methylheptanyl)-N-phenyl-2-(1,3-dioxan-2-yl)ethylsulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: N-phenyl-2-(1,3-dioxan-2-yl)ethylsulfonamide

: 4128-31-8,113301-48-7,4128-32-9
rac-octan-2-ol

: 874979-47-2
N-(1-methylheptanyl)-N-phenyl-2-(1,3-dioxan-2-yl)ethylsulfonamide

Guidance literature:: With cyanomethylenetributyl-phosphorane; In toluene; at 80 ℃; for 24h;
DOI:10.1021/ol052545+

Reference yield:

: 874979-34-7
2-[1,3]dioxan-2-yl-ethanesulfonyl chloride

: 874979-47-2
N-(1-methylheptanyl)-N-phenyl-2-(1,3-dioxan-2-yl)ethylsulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / Et₃N / CH₂Cl₂ / 0.83 h / 0 °C

2: 91 percent / (cyanomethylene)tributylphosphorane / toluene / 24 h / 80 °C

With triethylamine; cyanomethylenetributyl-phosphorane; In dichloromethane; toluene; 2: Mitsunobu alkylation;
DOI:10.1021/ol052545+

Reference yield:

: 13297-07-9
2-(2-chloroethyl)-1,3-dioxane

: 874979-47-2
N-(1-methylheptanyl)-N-phenyl-2-(1,3-dioxan-2-yl)ethylsulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: Na₂SO₃ / dimethylformamide; H₂O / 72 h / Heating

1.2: 83 percent / SO₂Cl₂; PPh₃ / CH₂Cl₂ / 2 h / 0 °C

2.1: 98 percent / Et₃N / CH₂Cl₂ / 0.83 h / 0 °C

3.1: 91 percent / (cyanomethylene)tributylphosphorane / toluene / 24 h / 80 °C

With triethylamine; cyanomethylenetributyl-phosphorane; sodium sulfite; In dichloromethane; water; N,N-dimethyl-formamide; toluene; 3.1: Mitsunobu alkylation;
DOI:10.1021/ol052545+