5-hydroxy-2-(4-hydroxybenzyl)-3-(4-hydroxyphenethyl)-1,4-bis(4-hydroxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-7-yl 2,2,2-trichloroethyl sulfate

Base Information

Chemical Name:5-hydroxy-2-(4-hydroxybenzyl)-3-(4-hydroxyphenethyl)-1,4-bis(4-hydroxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-7-yl 2,2,2-trichloroethyl sulfate
CAS No.:900504-67-8
Molecular Formula:C₄₃H₃₃Cl₃N₂O₉S
Molecular Weight:860.168
Hs Code.:

5-hydroxy-2-(4-hydroxybenzyl)-3-(4-hydroxyphenethyl)-1,4-bis(4-hydroxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-7-yl 2,2,2-trichloroethyl sulfate

Synonyms:5-hydroxy-2-(4-hydroxybenzyl)-3-(4-hydroxyphenethyl)-1,4-bis(4-hydroxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-7-yl 2,2,2-trichloroethyl sulfate

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Chemical Property of 5-hydroxy-2-(4-hydroxybenzyl)-3-(4-hydroxyphenethyl)-1,4-bis(4-hydroxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-7-yl 2,2,2-trichloroethyl sulfate

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Technology Process of 5-hydroxy-2-(4-hydroxybenzyl)-3-(4-hydroxyphenethyl)-1,4-bis(4-hydroxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-7-yl 2,2,2-trichloroethyl sulfate

There total 33 articles about 5-hydroxy-2-(4-hydroxybenzyl)-3-(4-hydroxyphenethyl)-1,4-bis(4-hydroxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-7-yl 2,2,2-trichloroethyl sulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 900504-66-7
5-methoxy-2-(4-methoxybenzyl)-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-7-yl 2,2,2-trichloroethyl sulfate

: 900504-67-8
5-hydroxy-2-(4-hydroxybenzyl)-3-(4-hydroxyphenethyl)-1,4-bis(4-hydroxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-7-yl 2,2,2-trichloroethyl sulfate

Guidance literature:: With boron trichloride; tetra-(n-butyl)ammonium iodide; In dichloromethane; at 0 - 20 ℃;
DOI:10.1002/asia.201000544

Reference yield:

: 900504-65-6
5-methoxy-2-(4-methoxybenzyl)-3-(4-methoxyphenethyl)-1,4-bis(4-methoxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-7-ol

: 900504-67-8
5-hydroxy-2-(4-hydroxybenzyl)-3-(4-hydroxyphenethyl)-1,4-bis(4-hydroxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-7-yl 2,2,2-trichloroethyl sulfate

Guidance literature:: Multi-step reaction with 2 steps

1: 109 mg / DABCO / tetrahydrofuran / 1 h

2: 85 percent / BCl₃; n-Bu₄NI / CH₂Cl₂ / 0.5 h / 0 °C

With 1,4-diaza-bicyclo[2.2.2]octane; boron trichloride; tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja0617800

Reference yield:

: 864816-24-0
7-isopropoxy-5-methoxy-1,4-bis-(4-methoxy-phenyl)-3-[2-(4-methoxy-phenyl)-ethyl]-3,6-dihydro-pyrrolo[2,3-c]carbazole

: 900504-67-8
5-hydroxy-2-(4-hydroxybenzyl)-3-(4-hydroxyphenethyl)-1,4-bis(4-hydroxyphenyl)-3,6-dihydropyrrolo[2,3-c]carbazol-7-yl 2,2,2-trichloroethyl sulfate

Guidance literature:: Multi-step reaction with 5 steps

1: 69 percent / NBS / tetrahydrofuran / 0.5 h / 0 °C

2: 90 percent / Pd(OAc)2; S-PHOS / dimethylformamide; tetrahydrofuran / 4.5 h / 110 °C

3: BCl₃ / CH₂Cl₂ / 1 h / -20 - 0 °C

4: 109 mg / DABCO / tetrahydrofuran / 1 h

5: 85 percent / BCl₃; n-Bu₄NI / CH₂Cl₂ / 0.5 h / 0 °C

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; 1,4-diaza-bicyclo[2.2.2]octane; palladium diacetate; N-Bromosuccinimide; boron trichloride; tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja0617800