2-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-cyclopent-1-enecarboxylic acid ethyl ester

Base Information

• Chemical Name: 2-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-cyclopent-1-enecarboxylic acid ethyl ester
• CAS No.: 1192170-61-8
• Molecular Formula: C₂₀H₃₀O₃Si
• Molecular Weight: 346.542

Synonyms:2-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-cyclopent-1-enecarboxylic acid ethyl ester

Chemical Property of 2-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-cyclopent-1-enecarboxylic acid ethyl ester

Chemical Property:

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Technology Process of 2-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-cyclopent-1-enecarboxylic acid ethyl ester

There total 1 articles about 2-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-cyclopent-1-enecarboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

2-trifluoromethanesulfonyloxy-cyclopent-1-enecarboxylic acid ethyl ester (122539-74-6) + (4-((tert-butyldimethylsilyl)oxy)phenyl)boronic acid (159191-56-7) → 2-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-cyclopent-1-enecarboxylic acid ethyl ester (1192170-61-8)

Guidance literature:

With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; for 5h; Reflux;

DOI:10.1021/ja9057103

Reference yield: 95.0%

2-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-cyclopent-1-enecarboxylic acid ethyl ester (1192170-61-8) → 2-(4-hydroxy-phenyl)-cyclopent-1-enecarboxylic acid ethyl ester (1192170-63-0)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1021/ja9057103

upstream raw materials:

2-trifluoromethanesulfonyloxy-cyclopent-1-enecarboxylic acid ethyl ester

(4-((tert-butyldimethylsilyl)oxy)phenyl)boronic acid

Downstream raw materials:

2-(4-hydroxy-phenyl)-cyclopent-1-enecarboxylic acid ethyl ester

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