ethyl 3-[2,2-dimethyl-4,6-dioxo-3-[(1S)-1-phenylethyl]-1,3-oxazinan-5-yl]-5-methyl-hexanoate

Base Information

Chemical Name:ethyl 3-[2,2-dimethyl-4,6-dioxo-3-[(1S)-1-phenylethyl]-1,3-oxazinan-5-yl]-5-methyl-hexanoate
CAS No.:1310495-06-7
Molecular Formula:C₂₃H₃₃NO₅
Molecular Weight:403.519
Hs Code.:

Synonyms:ethyl 3-[2,2-dimethyl-4,6-dioxo-3-[(1S)-1-phenylethyl]-1,3-oxazinan-5-yl]-5-methyl-hexanoate

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Chemical Property of ethyl 3-[2,2-dimethyl-4,6-dioxo-3-[(1S)-1-phenylethyl]-1,3-oxazinan-5-yl]-5-methyl-hexanoate

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Technology Process of ethyl 3-[2,2-dimethyl-4,6-dioxo-3-[(1S)-1-phenylethyl]-1,3-oxazinan-5-yl]-5-methyl-hexanoate

There total 1 articles about ethyl 3-[2,2-dimethyl-4,6-dioxo-3-[(1S)-1-phenylethyl]-1,3-oxazinan-5-yl]-5-methyl-hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34993-63-0,79918-80-2,2351-89-5
5-methyl-2-hexenoic acid ethyl ester

: 1310495-05-6
2,2-dimethyl-3-[(1S)-1-phenylethyl]-1,3-oxazinane-4,6-dione

: 1310495-06-7
ethyl 3-[2,2-dimethyl-4,6-dioxo-3-[(1S)-1-phenylethyl]-1,3-oxazinan-5-yl]-5-methyl-hexanoate

Guidance literature:: With triethylamine; In dichloromethane; Reflux;

Reference yield:

: 1310495-06-7
ethyl 3-[2,2-dimethyl-4,6-dioxo-3-[(1S)-1-phenylethyl]-1,3-oxazinan-5-yl]-5-methyl-hexanoate

: 148553-50-8
pregabilin

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium chloride / water; dimethyl sulfoxide / 8 h / 145 - 155 °C

2.1: hydrazine hydrate / ethanol / 4 h / Reflux

3.1: hydrogenchloride; sodium nitrite / water / 1.5 h / 55 - 60 °C

3.2: pH 12

4.1: water; hydrogen bromide / 5 h / 100 - 110 °C

With hydrogenchloride; water; hydrogen bromide; hydrazine hydrate; sodium chloride; sodium nitrite; In ethanol; water; dimethyl sulfoxide;