2-(diphenylacetyl)-4-methyl-6,6-diphenyl-2-azatricyclo(5.2.2.0 1,5)undeca-4,8,10-trien-3-one

Base Information

Chemical Name:2-(diphenylacetyl)-4-methyl-6,6-diphenyl-2-azatricyclo(5.2.2.0 1,5)undeca-4,8,10-trien-3-one
CAS No.:108832-92-4
Molecular Formula:C₃₇H₂₉NO₂
Molecular Weight:519.643
Hs Code.:

Synonyms:2-(diphenylacetyl)-4-methyl-6,6-diphenyl-2-azatricyclo(5.2.2.0 1,5)undeca-4,8,10-trien-3-one

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Chemical Property of 2-(diphenylacetyl)-4-methyl-6,6-diphenyl-2-azatricyclo(5.2.2.0 1,5)undeca-4,8,10-trien-3-one

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Technology Process of 2-(diphenylacetyl)-4-methyl-6,6-diphenyl-2-azatricyclo(5.2.2.0 1,5)undeca-4,8,10-trien-3-one

There total 1 articles about 2-(diphenylacetyl)-4-methyl-6,6-diphenyl-2-azatricyclo(5.2.2.0 1,5)undeca-4,8,10-trien-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 14181-84-1
triphenylketeneimine

: 6002-06-8
2-methyl-4,4-diphenylbuta-2,3-dienoic acid

: 108832-92-4
2-(diphenylacetyl)-4-methyl-6,6-diphenyl-2-azatricyclo(5.2.2.0 1,5)undeca-4,8,10-trien-3-one

Guidance literature:: In tetrahydrofuran; at 90 ℃; for 18h;
DOI:10.1002/hlca.19870700130

Reference yield: 44.0%

: 13463-40-6,37220-42-1
iron pentacarbonyl

: 108832-92-4
2-(diphenylacetyl)-4-methyl-6,6-diphenyl-2-azatricyclo(5.2.2.0 1,5)undeca-4,8,10-trien-3-one

: 124720-34-9
{2-(2,2-diphenylacetyl)-4-methyl-6,6-diphenyl-2-azatricyclo{5.2.2.0(1,5)}undeca-4,8,10-trien-3-one}tricarbonyliron

Guidance literature:: In tetrahydrofuran; Irradiation (UV/VIS); Irradn. of a soln. of hydrobarrelene and Fe-complex with 50-W high pressure Hg lamp under N2 for 3 h.; Evapn. of solvent, preparative TLC (petroleum ether/AcOEt/acetone).;
DOI:10.1002/hlca.19890720404