[Ir(NH₂NHC₆H₂(Cl)NO)Cl(CO)[P(C₆H₅)3]2]⁽¹⁺⁾*BF₄^(1-)=[Ir(NH₂NHC₆H₂(Cl)NO)Cl(CO)[P(C₆H₅)3]2][BF₄]

Base Information

• Chemical Name: [Ir(NH₂NHC₆H₂(Cl)NO)Cl(CO)[P(C₆H₅)3]2]⁽¹⁺⁾*BF₄^(1-)=[Ir(NH₂NHC₆H₂(Cl)NO)Cl(CO)[P(C₆H₅)3]2][BF₄]
• CAS No.: 85837-45-2
• Molecular Formula: BF₄*C₄₃H₃₅Cl₂IrN₃O₂P₂
• Molecular Weight: 1037.65

Synonyms:[Ir(NH₂NHC₆H₂(Cl)NO)Cl(CO)[P(C₆H₅)3]2]⁽¹⁺⁾*BF₄^(1-)=[Ir(NH₂NHC₆H₂(Cl)NO)Cl(CO)[P(C₆H₅)3]2][BF₄]

Chemical Property of [Ir(NH₂NHC₆H₂(Cl)NO)Cl(CO)[P(C₆H₅)3]2]⁽¹⁺⁾*BF₄^(1-)=[Ir(NH₂NHC₆H₂(Cl)NO)Cl(CO)[P(C₆H₅)3]2][BF₄]

Chemical Property:

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Technology Process of [Ir(NH₂NHC₆H₂(Cl)NO)Cl(CO)[P(C₆H₅)3]2]⁽¹⁺⁾*BF₄^(1-)=[Ir(NH₂NHC₆H₂(Cl)NO)Cl(CO)[P(C₆H₅)3]2][BF₄]

There total 3 articles about [Ir(NH₂NHC₆H₂(Cl)NO)Cl(CO)[P(C₆H₅)3]2]⁽¹⁺⁾*BF₄^(1-)=[Ir(NH₂NHC₆H₂(Cl)NO)Cl(CO)[P(C₆H₅)3]2][BF₄] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

[Ir(NHNHC6H3NO2-o)(CO)(PPh3)2][BF4] → [Ir(NH2NHC6H2(Cl)NO)Cl(CO)[P(C6H5)3]2](1+)*BF4(1-)=[Ir(NH2NHC6H2(Cl)NO)Cl(CO)[P(C6H5)3]2][BF4] (85837-45-2)

Guidance literature:

With HCl; cooling to -195.8°C under N2 in a Shclenk tube, condensing of dry HCl gas, stirring at -110°C for a few minutes; pumping off HCl, washing with water three times, pptn. with acetone/hexane, elem. anal.;

DOI:10.1016/S0022-328X(00)98635-2

Reference yield:

[Ir(NH2NHC6H3NO2)Cl(CO)[P(C6H5)3]2](1+)*BF4(1-)=[Ir(NH2NHC6H3NO2)Cl(CO)[P(C6H5)3]2][BF4] (85837-43-0) → [Ir(NH2NHC6H2(Cl)NO)Cl(CO)[P(C6H5)3]2](1+)*BF4(1-)=[Ir(NH2NHC6H2(Cl)NO)Cl(CO)[P(C6H5)3]2][BF4] (85837-45-2)

Guidance literature:

With HCl; liq. HCl action;

DOI:10.1016/S0022-328X(00)98635-2

Reference yield:

tetrafluoroboric acid + Ir(NHNHC6H2(Cl)NO)Cl(CO)[P(C6H5)3]2 (85837-46-3) → [Ir(NH2NHC6H2(Cl)NO)Cl(CO)[P(C6H5)3]2](1+)*BF4(1-)=[Ir(NH2NHC6H2(Cl)NO)Cl(CO)[P(C6H5)3]2][BF4] (85837-45-2)

Guidance literature:

DOI:10.1016/S0022-328X(00)98635-2

upstream raw materials:

[Ir(NH₂NHC₆H₃NO₂)Cl(CO)[P(C₆H₅)3]2]⁽¹⁺⁾*BF₄^(1-)=[Ir(NH₂NHC₆H₃NO₂)Cl(CO)[P(C₆H₅)3]2][BF₄]

Ir(NHNHC₆H₂(Cl)NO)Cl(CO)[P(C₆H₅)3]2

Downstream raw materials:

Ir(NHNHC₆H₂(Cl)NO)Cl(CO)[P(C₆H₅)3]2

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