Technology Process of C14H14ClN3O6S2
There total 5 articles about C14H14ClN3O6S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C14H14ClN3O4S2;
With
3-chloro-benzenecarboperoxoic acid;
In
chloroform;
for 0.25h;
Reflux;
With
sodium hydrogencarbonate;
In
chloroform; water;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: pyridine / dichloromethane / 1.25 h / 20 °C / Cooling with ice; Inert atmosphere
2: 1,1'-azodicarbonyl-dipiperidine; triphenylphosphine / tetrahydrofuran / 3.25 h / 0 - 20 °C
3: potassium carbonate; ethanol / 1 h / Reflux
4: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / 20 °C / Cooling with ice; Inert atmosphere
5: 3-chloro-benzenecarboperoxoic acid / chloroform / 0.25 h / Reflux
With
pyridine; ethanol; sodium hexamethyldisilazane; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; 1,1'-azodicarbonyl-dipiperidine;
In
tetrahydrofuran; dichloromethane; chloroform;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1,1'-azodicarbonyl-dipiperidine; triphenylphosphine / tetrahydrofuran / 3.25 h / 0 - 20 °C
2: potassium carbonate; ethanol / 1 h / Reflux
3: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / 20 °C / Cooling with ice; Inert atmosphere
4: 3-chloro-benzenecarboperoxoic acid / chloroform / 0.25 h / Reflux
With
ethanol; sodium hexamethyldisilazane; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; 1,1'-azodicarbonyl-dipiperidine;
In
tetrahydrofuran; chloroform;
