methyl 4-<<6-amino>indol-1-yl>methyl>-3-methoxybenzoate

Base Information

Chemical Name:methyl 4-<<6-amino>indol-1-yl>methyl>-3-methoxybenzoate
CAS No.:104435-96-3
Molecular Formula:C₂₄H₂₆N₂O₅
Molecular Weight:422.481
Hs Code.:

methyl 4-<<6-<N-<(cyclopentyloxy)carbonyl>amino>indol-1-yl>methyl>-3-methoxybenzoate

Synonyms:methyl 4-<<6-amino>indol-1-yl>methyl>-3-methoxybenzoate

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Chemical Property of methyl 4-<<6-amino>indol-1-yl>methyl>-3-methoxybenzoate

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Technology Process of methyl 4-<<6-amino>indol-1-yl>methyl>-3-methoxybenzoate

There total 6 articles about methyl 4-<<6-amino>indol-1-yl>methyl>-3-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3556-83-0
methyl 4-methyl-3-methoxybenzoate

: 104435-96-3
methyl 4-<<6-amino>indol-1-yl>methyl>-3-methoxybenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 64 percent / bromine / CCl₄ / 4 h / Irradiation

2: 95 percent / K₂CO₃ / acetone / 48 h / Heating

3: 95 percent / acetic acid-EtOAc, H₂ / 10percent Pd/C / 24 h / 2585.7 Torr

4: 2.) Et₃N / 1.) dioxane, RT, 30 min, 2.) 80 deg C, 2.5 h

With hydrogen; bromine; potassium carbonate; acetic acid; ethyl acetate; triethylamine; palladium on activated charcoal; In tetrachloromethane; acetone;
DOI:10.1021/jm00168a036

Reference yield:

: 7151-68-0
3-methoxy-p-toluic acid

: 104435-96-3
methyl 4-<<6-amino>indol-1-yl>methyl>-3-methoxybenzoate

Guidance literature:: Multi-step reaction with 5 steps

1: 98 percent / acetyl chloride / 36 h

2: 64 percent / bromine / CCl₄ / 4 h / Irradiation

3: 95 percent / K₂CO₃ / acetone / 48 h / Heating

4: 95 percent / acetic acid-EtOAc, H₂ / 10percent Pd/C / 24 h / 2585.7 Torr

5: 2.) Et₃N / 1.) dioxane, RT, 30 min, 2.) 80 deg C, 2.5 h

With hydrogen; bromine; potassium carbonate; acetic acid; ethyl acetate; triethylamine; acetyl chloride; palladium on activated charcoal; In tetrachloromethane; acetone;
DOI:10.1021/jm00168a036

Reference yield:

: 70264-94-7
methyl 4-(bromomethyl)-3-methoxybenzoate

: 104435-96-3
methyl 4-<<6-amino>indol-1-yl>methyl>-3-methoxybenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / K₂CO₃ / acetone / 48 h / Heating

2: 95 percent / acetic acid-EtOAc, H₂ / 10percent Pd/C / 24 h / 2585.7 Torr

3: 2.) Et₃N / 1.) dioxane, RT, 30 min, 2.) 80 deg C, 2.5 h

With hydrogen; potassium carbonate; acetic acid; ethyl acetate; triethylamine; palladium on activated charcoal; In acetone;
DOI:10.1021/jm00168a036