C₄₀H₂₄N₄O₄Zn

Base Information

• Chemical Name: C₄₀H₂₄N₄O₄Zn
• CAS No.: 1296165-45-1
• Molecular Formula: C₄₀H₂₄N₄O₄Zn
• Molecular Weight: 690.045
• Mol file: 1296165-45-1.mol

Synonyms:C₄₀H₂₄N₄O₄Zn

Chemical Property of C₄₀H₂₄N₄O₄Zn

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₀H₂₄N₄O₄Zn

There total 5 articles about C₄₀H₂₄N₄O₄Zn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

C46H40N4O4Si2Zn (1296165-44-0) → C40H24N4O4Zn (1296165-45-1)

Guidance literature:

With tetrabutyl ammonium fluoride; In dichloromethane; at 25 ℃; for 0.5h;

DOI:10.1039/c1cc00112d

Reference yield:

C36H24N4O4Zn (205177-64-6) → C40H24N4O4Zn (1296165-45-1)

Guidance literature:

Multi-step reaction with 3 steps

1: N-Bromosuccinimide / methanol; dichloromethane / 0.5 h / 25 °C

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 16 h / 25 °C / Inert atmosphere

3: tetrabutyl ammonium fluoride / dichloromethane / 0.5 h / 25 °C

With bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; copper(l) iodide; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; methanol; dichloromethane;

DOI:10.1039/c1cc00112d

Reference yield:

C36H22Br2N4O4Zn (1296165-43-9) → C40H24N4O4Zn (1296165-45-1)

Guidance literature:

Multi-step reaction with 2 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / tetrahydrofuran / 16 h / 25 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / dichloromethane / 0.5 h / 25 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1039/c1cc00112d

upstream raw materials:

di(pyrrol-2-yl)methane

C₄₆H₄₀N₄O₄Si₂Zn

C₃₆H₂₄N₄O₄Zn

C₃₆H₂₂Br₂N₄O₄Zn

Downstream raw materials:

C₁₃₂H₉₆N₁₂O₈Zn₂