tert-butyl (5S,6R)-5-(benzyloxy)-6-methyl-2-oxo-5,6-dihydropyridine-1(2H)-carboxylate

Base Information

Chemical Name:tert-butyl (5S,6R)-5-(benzyloxy)-6-methyl-2-oxo-5,6-dihydropyridine-1(2H)-carboxylate
CAS No.:1200404-59-6
Molecular Formula:C₁₈H₂₃NO₄
Molecular Weight:317.385
Hs Code.:

Synonyms:tert-butyl (5S,6R)-5-(benzyloxy)-6-methyl-2-oxo-5,6-dihydropyridine-1(2H)-carboxylate

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Chemical Property of tert-butyl (5S,6R)-5-(benzyloxy)-6-methyl-2-oxo-5,6-dihydropyridine-1(2H)-carboxylate

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Technology Process of tert-butyl (5S,6R)-5-(benzyloxy)-6-methyl-2-oxo-5,6-dihydropyridine-1(2H)-carboxylate

There total 1 articles about tert-butyl (5S,6R)-5-(benzyloxy)-6-methyl-2-oxo-5,6-dihydropyridine-1(2H)-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1200404-70-1
tert-butyl (2R,3S)-3-(benzyloxy)-2-methyl-6-oxopiperidine-1-carboxylate

: 1200404-59-6
tert-butyl (5S,6R)-5-(benzyloxy)-6-methyl-2-oxo-5,6-dihydropyridine-1(2H)-carboxylate

Guidance literature:: tert-butyl (2R,3S)-3-(benzyloxy)-2-methyl-6-oxopiperidine-1-carboxylate; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃;

With Phenylselenyl bromide; In tetrahydrofuran; at -78 ℃;

With dihydrogen peroxide; In dichloromethane; water; for 3h;
DOI:10.1016/j.tet.2009.09.083

Reference yield: 92.0%

: 1200404-59-6
tert-butyl (5S,6R)-5-(benzyloxy)-6-methyl-2-oxo-5,6-dihydropyridine-1(2H)-carboxylate

: 1200404-72-3
tert-butyl (1S,4R,5R,6S)-5-(benzyloxy)-4-methyl-2-oxo-7-oxa-3-azabicyclo[4.1.0]heptane-3-carboxylate

Guidance literature:: tert-butyl (5S,6R)-5-(benzyloxy)-6-methyl-2-oxo-5,6-dihydropyridine-1(2H)-carboxylate; With tert.-butylhydroperoxide; potassium carbonate; In nonane; N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; nonane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2009.09.083

Reference yield:

: 1200404-59-6
tert-butyl (5S,6R)-5-(benzyloxy)-6-methyl-2-oxo-5,6-dihydropyridine-1(2H)-carboxylate

: 1200404-80-3
tert-butyl (2R,3R,4R,5S)-3-(benzyloxy)-4,5-dihydroxy-2-methyl-6-oxopiperidine-1-carboxylate

Guidance literature:: tert-butyl (5S,6R)-5-(benzyloxy)-6-methyl-2-oxo-5,6-dihydropyridine-1(2H)-carboxylate; With osmium(VIII) oxide; 4-methylmorpholine N-oxide; citric acid; In water; tert-butyl alcohol; at 20 ℃; for 20h;

With sodium sulfite; In water; tert-butyl alcohol;
DOI:10.1016/j.tet.2009.09.083