Technology Process of C42H37N5O7
There total 5 articles about C42H37N5O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
2,6-di-tert-butyl-4-methylpyridine;
In
dichloromethane; N,N-dimethyl-formamide;
at 0 ℃;
for 0.666667h;
regioselective reaction;
DOI:10.1002/asia.201000828
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 5%-palladium/activated carbon; hydrogen / ethanol; ethyl acetate / 2 h / 20 °C
2: benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane; N,N-dimethyl-formamide / 48 h / 20 °C
3: trifluoroacetic acid / tetrahydrofuran; water / 5 - 20 °C
4: 2,6-di-tert-butyl-4-methylpyridine / dichloromethane; N,N-dimethyl-formamide / 0.67 h / 0 °C
With
2,6-di-tert-butyl-4-methylpyridine; 5%-palladium/activated carbon; hydrogen; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; trifluoroacetic acid;
In
tetrahydrofuran; ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1002/asia.201000828
- Guidance literature:
-
Multi-step reaction with 3 steps
1: benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane; N,N-dimethyl-formamide / 48 h / 20 °C
2: trifluoroacetic acid / tetrahydrofuran; water / 5 - 20 °C
3: 2,6-di-tert-butyl-4-methylpyridine / dichloromethane; N,N-dimethyl-formamide / 0.67 h / 0 °C
With
2,6-di-tert-butyl-4-methylpyridine; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/asia.201000828