5-[4-(4-Carboxy-4-methyl-pentyloxy)-2,5-dimethyl-phenylsulfanyl]-2,2-dimethyl-pentanoic acid

Base Information

Chemical Name:5-[4-(4-Carboxy-4-methyl-pentyloxy)-2,5-dimethyl-phenylsulfanyl]-2,2-dimethyl-pentanoic acid
CAS No.:85629-75-0
Molecular Formula:C₂₂H₃₄O₅S
Molecular Weight:410.575
Hs Code.:

Synonyms:5-[4-(4-Carboxy-4-methyl-pentyloxy)-2,5-dimethyl-phenylsulfanyl]-2,2-dimethyl-pentanoic acid

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Chemical Property of 5-[4-(4-Carboxy-4-methyl-pentyloxy)-2,5-dimethyl-phenylsulfanyl]-2,2-dimethyl-pentanoic acid

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Technology Process of 5-[4-(4-Carboxy-4-methyl-pentyloxy)-2,5-dimethyl-phenylsulfanyl]-2,2-dimethyl-pentanoic acid

There total 3 articles about 5-[4-(4-Carboxy-4-methyl-pentyloxy)-2,5-dimethyl-phenylsulfanyl]-2,2-dimethyl-pentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79520-52-8
5-Bromo-2,2-dimethylpentanoic acid,methyl ester

: 85629-75-0
5-[4-(4-Carboxy-4-methyl-pentyloxy)-2,5-dimethyl-phenylsulfanyl]-2,2-dimethyl-pentanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, RT, 1 h, 2.) DMF, 80 - 85 deg C, 12 - 14 h

2: 2 N NaOH / methanol / 3 h / Heating

With sodium hydroxide; sodium hydride; In methanol;
DOI:10.1021/jm00361a015

Reference yield:

: 5-[4-(4-Methoxycarbonyl-4-methyl-pentyloxy)-2,5-dimethyl-phenylsulfanyl]-2,2-dimethyl-pentanoic acid methyl ester

: 85629-75-0
5-[4-(4-Carboxy-4-methyl-pentyloxy)-2,5-dimethyl-phenylsulfanyl]-2,2-dimethyl-pentanoic acid

Guidance literature:: With sodium hydroxide; In methanol; for 3h; Yield given; Heating;
DOI:10.1021/jm00361a015

Reference yield:

: 106949-90-0
2,5-dimethyl-4-hydroxy-mercaptobenzene

: 85629-75-0
5-[4-(4-Carboxy-4-methyl-pentyloxy)-2,5-dimethyl-phenylsulfanyl]-2,2-dimethyl-pentanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, RT, 1 h, 2.) DMF, 80 - 85 deg C, 12 - 14 h

2: 2 N NaOH / methanol / 3 h / Heating

With sodium hydroxide; sodium hydride; In methanol;
DOI:10.1021/jm00361a015