(4R,5S)-4-((3,4-dimethoxybenzyl)oxy)-5-(2-iodoethyl)-2,2-dimethyltetrahydrofuran

Base Information

Chemical Name:(4R,5S)-4-((3,4-dimethoxybenzyl)oxy)-5-(2-iodoethyl)-2,2-dimethyltetrahydrofuran
CAS No.:1162782-20-8
Molecular Formula:C₁₇H₂₅IO₄
Molecular Weight:420.288
Hs Code.:

Synonyms:(4R,5S)-4-((3,4-dimethoxybenzyl)oxy)-5-(2-iodoethyl)-2,2-dimethyltetrahydrofuran

Suppliers and Price of (4R,5S)-4-((3,4-dimethoxybenzyl)oxy)-5-(2-iodoethyl)-2,2-dimethyltetrahydrofuran

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4R,5S)-4-((3,4-dimethoxybenzyl)oxy)-5-(2-iodoethyl)-2,2-dimethyltetrahydrofuran

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Technology Process of (4R,5S)-4-((3,4-dimethoxybenzyl)oxy)-5-(2-iodoethyl)-2,2-dimethyltetrahydrofuran

There total 1 articles about (4R,5S)-4-((3,4-dimethoxybenzyl)oxy)-5-(2-iodoethyl)-2,2-dimethyltetrahydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1162782-19-5
2-((2S,3R)-3-((3,4-dimethoxybenzyl)oxy)-5,5-dimethyltetrahydro-2-furanyl)ethanol

: 1162782-20-8
(4R,5S)-4-((3,4-dimethoxybenzyl)oxy)-5-(2-iodoethyl)-2,2-dimethyltetrahydrofuran

Guidance literature:: With 1H-imidazole; iodine; triphenylphosphine; In diethyl ether; acetonitrile; at 0 ℃; Inert atmosphere;
DOI:10.1002/chem.200802069

Reference yield:

: 1162782-20-8
(4R,5S)-4-((3,4-dimethoxybenzyl)oxy)-5-(2-iodoethyl)-2,2-dimethyltetrahydrofuran

: C₂₆H₄₂BO₅^(1-)*Li⁽¹⁺⁾

Guidance literature:: (4R,5S)-4-((3,4-dimethoxybenzyl)oxy)-5-(2-iodoethyl)-2,2-dimethyltetrahydrofuran; With tert.-butyl lithium; In tetrahydrofuran; diethyl ether; pentane; at -78 ℃; Inert atmosphere;

With 9-methoxy-9-borabicyclo[3.3.1]nonane; In tetrahydrofuran; diethyl ether; pentane; at -78 - 20 ℃; for 1.08333h; Inert atmosphere;
DOI:10.1002/chem.200802069