3''-N-acetyl-1-deamino-1-oxo-3,2',6'-tris-N-(2,2,2-trichloroethoxycarbonyl)gentamicin C_1a

Base Information

• Chemical Name: 3''-N-acetyl-1-deamino-1-oxo-3,2',6'-tris-N-(2,2,2-trichloroethoxycarbonyl)gentamicin C_1a
• CAS No.: 66065-93-8
• Molecular Formula: C₃₀H₄₁Cl₉N₄O₁₅
• Molecular Weight: 1016.75

Synonyms:3''-N-acetyl-1-deamino-1-oxo-3,2',6'-tris-N-(2,2,2-trichloroethoxycarbonyl)gentamicin C_1a

Chemical Property of 3''-N-acetyl-1-deamino-1-oxo-3,2',6'-tris-N-(2,2,2-trichloroethoxycarbonyl)gentamicin C_1a

Chemical Property:

Purity/Quality:

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Technology Process of 3''-N-acetyl-1-deamino-1-oxo-3,2',6'-tris-N-(2,2,2-trichloroethoxycarbonyl)gentamicin C_1a

There total 2 articles about 3''-N-acetyl-1-deamino-1-oxo-3,2',6'-tris-N-(2,2,2-trichloroethoxycarbonyl)gentamicin C_1a which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

3''-N-acetyl-3,2',6'-tris-N-(2,2,2-trichloroethoxycarbonyl)gentamicin C1a (66065-88-1) → 3''-N-acetyl-1-deamino-1-oxo-3,2',6'-tris-N-(2,2,2-trichloroethoxycarbonyl)gentamicin C1a (66065-93-8)

Guidance literature:

With 3,5-di-tert-butyl-o-benzoquinone; oxalic acid; In methanol; at 25 ℃; 1.) 16 h, 2.) pH = 3, tetrahydrofuran, water, 24 h;

DOI:10.1039/P19810002168

Reference yield:

3,2',6'-tris-N-(2,2,2-trichloroethoxycarbonyl)gentamicin C1a (66065-87-0) → 3''-N-acetyl-1-deamino-1-oxo-3,2',6'-tris-N-(2,2,2-trichloroethoxycarbonyl)gentamicin C1a (66065-93-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / tetrahydrofuran; H₂O / 65 h / 25 °C

2: 94 percent / 3,5-di-t-butyl-1,2-benzoquinone, oxalic acid / methanol / 25 °C / 1.) 16 h, 2.) pH = 3, tetrahydrofuran, water, 24 h

With 3,5-di-tert-butyl-o-benzoquinone; oxalic acid; In tetrahydrofuran; methanol; water;

DOI:10.1039/P19810002168

upstream raw materials:

3''-N-acetyl-3,2',6'-tris-N-(2,2,2-trichloroethoxycarbonyl)gentamicin C_1a

3,2',6'-tris-N-(2,2,2-trichloroethoxycarbonyl)gentamicin C_1a

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