Technology Process of C29H30N6O5S
There total 4 articles about C29H30N6O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
pyridine; acetic anhydride;
at 70 ℃;
for 4.5h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: nitric acid; sulfur trioxide; sulfuric acid / 28.5 h / 55 - 80 °C
1.2: Cooling with ice
2.1: hydrogenchloride; tin / water; methanol / 8 h / 75 °C
3.1: sulfuric acid; nitrosylsulfuric acid / water; acetic acid / 3.25 h / 2 °C
3.2: 1 h / 3 - 6 °C / pH 1.45 - 2
4.1: acetic anhydride; pyridine / 4.5 h / 70 °C
With
hydrogenchloride; tin; nitrosylsulfuric acid; sulfuric acid; sulfur trioxide; nitric acid;
In
pyridine; methanol; water; acetic anhydride; acetic acid;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogenchloride; tin / water; methanol / 8 h / 75 °C
2.1: sulfuric acid; nitrosylsulfuric acid / water; acetic acid / 3.25 h / 2 °C
2.2: 1 h / 3 - 6 °C / pH 1.45 - 2
3.1: acetic anhydride; pyridine / 4.5 h / 70 °C
With
hydrogenchloride; tin; nitrosylsulfuric acid; sulfuric acid;
In
pyridine; methanol; water; acetic anhydride; acetic acid;