tert-butyl 3-phenethyl-2-(3-phenylprop-2-ynyl)-2H-azirine-2-carboxylate

Base Information

Chemical Name:tert-butyl 3-phenethyl-2-(3-phenylprop-2-ynyl)-2H-azirine-2-carboxylate
CAS No.:1627205-41-7
Molecular Formula:C₂₄H₂₅NO₂
Molecular Weight:359.468
Hs Code.:

Synonyms:tert-butyl 3-phenethyl-2-(3-phenylprop-2-ynyl)-2H-azirine-2-carboxylate

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Chemical Property of tert-butyl 3-phenethyl-2-(3-phenylprop-2-ynyl)-2H-azirine-2-carboxylate

Chemical Property:

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Technology Process of tert-butyl 3-phenethyl-2-(3-phenylprop-2-ynyl)-2H-azirine-2-carboxylate

There total 5 articles about tert-butyl 3-phenethyl-2-(3-phenylprop-2-ynyl)-2H-azirine-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1641546-18-0
C₂₄H₂₆O₃

: 1627205-41-7
tert-butyl 3-phenethyl-2-(3-phenylprop-2-ynyl)-2H-azirine-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; hydroxylamine hydrochloride / 50 °C

2: pyridine / dichloromethane / 20 °C / Inert atmosphere

3: triethylamine

With pyridine; hydroxylamine hydrochloride; triethylamine; In dichloromethane;
DOI:10.1002/anie.201402470

Reference yield:

: 540-88-5
acetic acid tert-butyl ester

: 1627205-41-7
tert-butyl 3-phenethyl-2-(3-phenylprop-2-ynyl)-2H-azirine-2-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium; diisopropylamine / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

1.2: 8 h / 20 °C

2.1: n-butyllithium; diisopropylamine / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

2.2: 12 h / Inert atmosphere

3.1: pyridine; hydroxylamine hydrochloride / 50 °C

4.1: pyridine / dichloromethane / 20 °C / Inert atmosphere

5.1: triethylamine

With pyridine; n-butyllithium; hydroxylamine hydrochloride; triethylamine; diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.201402470

Reference yield:

: 1794-48-5
1-bromo-3-phenylprop-2-yne

: 1627205-41-7
tert-butyl 3-phenethyl-2-(3-phenylprop-2-ynyl)-2H-azirine-2-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium; diisopropylamine / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

1.2: 8 h / 20 °C

2.1: n-butyllithium; diisopropylamine / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

2.2: 12 h / Inert atmosphere

3.1: pyridine; hydroxylamine hydrochloride / 50 °C

4.1: pyridine / dichloromethane / 20 °C / Inert atmosphere

5.1: triethylamine

With pyridine; n-butyllithium; hydroxylamine hydrochloride; triethylamine; diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.201402470