N⁴-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>tubercidylyl-(2'-> 5')-N⁴-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin Triethylammoniumsalz

Base Information

• Chemical Name: N⁴-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>tubercidylyl-(2'-> 5')-N⁴-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin Triethylammoniumsalz
• CAS No.: 90358-12-6
• Molecular Formula: C₆H₁₅N*C₅₄H₇₇N₈O₁₂PSi₃
• Molecular Weight: 1246.67

Synonyms:N⁴-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>tubercidylyl-(2'-> 5')-N⁴-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin Triethylammoniumsalz

Chemical Property of N⁴-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>tubercidylyl-(2'-> 5')-N⁴-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin Triethylammoniumsalz

Chemical Property:

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Technology Process of N⁴-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>tubercidylyl-(2'-> 5')-N⁴-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin Triethylammoniumsalz

There total 4 articles about N⁴-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>tubercidylyl-(2'-> 5')-N⁴-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin Triethylammoniumsalz which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

N4-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-P-methyltubercidylyl-(2'-> 5')-N4-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin (90373-53-8) + triethylamine (121-44-8) → N4-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>tubercidylyl-(2'-> 5')-N4-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin Triethylammoniumsalz (90358-12-6)

Guidance literature:

With thiophenol; In 1,4-dioxane; for 0.75h; Ambient temperature;

Reference yield:

5'-O-<(p-Anisyl)diphenylmethyl>-N4-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-P-methyltubercidylyl-(2'-> 5')-N4-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin (90358-07-9) → N4-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>tubercidylyl-(2'-> 5')-N4-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin Triethylammoniumsalz (90358-12-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 77 percent / ZnBr₂ / nitromethane; methanol / 0.08 h

2: 98 percent / thiophenol / dioxane / 0.75 h / Ambient temperature

With thiophenol; zinc dibromide; In 1,4-dioxane; methanol; nitromethane;

Reference yield:

Phosphorochloridous acid (2R,3R,4R,5R)-2-(4-benzoylamino-pyrrolo[2,3-d]pyrimidin-7-yl)-4-(tert-butyl-dimethyl-silanyloxy)-5-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-tetrahydro-furan-3-yl ester methyl ester → N4-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>tubercidylyl-(2'-> 5')-N4-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin Triethylammoniumsalz (90358-12-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 2.) I₂/H₂O / 1.) THF, 1 h, -78 deg C; 1 h, room temp, 2.) THF/sym-collidine, 15 min room temp

2: 77 percent / ZnBr₂ / nitromethane; methanol / 0.08 h

3: 98 percent / thiophenol / dioxane / 0.75 h / Ambient temperature

With water; iodine; thiophenol; zinc dibromide; In 1,4-dioxane; methanol; nitromethane;

upstream raw materials:

N⁴-Benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-P-methyltubercidylyl-(2'-> 5')-N⁴-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin

triethylamine

5'-O-<(p-Anisyl)diphenylmethyl>-N⁴-benzoyl-3'-O-<(tert-butyl)dimethylsilyl>-P-methyltubercidylyl-(2'-> 5')-N⁴-benzoyl-2',3'-bis-O-<(tert-butyl)dimethylsilyl>tubercidin

N⁴-Benzoyl-3'-O-(tert-butylsilyl)-5'-O-<(4-methoxyphenyl)(diphenyl)methyl>tubercidin

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