(3-oxapentane-1,5-dithiolato)(p-carbmethoxybenzenethiolato)(triphenylphosphine)-technetium(III)

Base Information

Chemical Name:(3-oxapentane-1,5-dithiolato)(p-carbmethoxybenzenethiolato)(triphenylphosphine)-technetium(III)
CAS No.:128337-28-0
Molecular Formula:C₃₀H₃₀O₃PS₃Tc
Molecular Weight:663.645
Hs Code.:

Synonyms:(3-oxapentane-1,5-dithiolato)(p-carbmethoxybenzenethiolato)(triphenylphosphine)-technetium(III)

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Chemical Property of (3-oxapentane-1,5-dithiolato)(p-carbmethoxybenzenethiolato)(triphenylphosphine)-technetium(III)

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Technology Process of (3-oxapentane-1,5-dithiolato)(p-carbmethoxybenzenethiolato)(triphenylphosphine)-technetium(III)

There total 2 articles about (3-oxapentane-1,5-dithiolato)(p-carbmethoxybenzenethiolato)(triphenylphosphine)-technetium(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 126600-70-2
(3-oxapentane-1,5-dithiolato)(p-carbmethoxybenzenethiolato)oxotechnetium(V)

: 128337-28-0
(3-oxapentane-1,5-dithiolato)(p-carbmethoxybenzenethiolato)(triphenylphosphine)-technetium(III)

Guidance literature:: With acetic acid; triphenylphosphine; In acetone; dissolving of Tc-compd. and phosphine in acetone, addn. of CH3COOH and stirring at room temp. for 45 min; reducing of volume until the soln. is turbid, standing in the refrigerator overnight, dissolving of ppt. in CHCl3 and addn. of MeOH;
DOI:10.1016/S0020-1693(00)88010-X

Reference yield: 40.0%

: 111821-29-5
tetrachlorobis(triphenylphosphine)technetium(IV)

: 6302-65-4
methyl 4-mercaptobenzoate

: 2150-02-9
bis(2-mercaptoethyl)ether

: 128337-28-0
(3-oxapentane-1,5-dithiolato)(p-carbmethoxybenzenethiolato)(triphenylphosphine)-technetium(III)

Guidance literature:: In ethanol; refluxing of a mixt. of Tc-compd., dithiol and thiol in ethanol for 2 h; reducing of volume, then standing overnight in the refrigerator, dissolving of ppt. in CHCl3 and addn. of MeOH, elem. anal.;
DOI:10.1016/S0020-1693(00)88010-X