all-trans-retinal propylene dithioacetal

Base Information

Chemical Name:all-trans-retinal propylene dithioacetal
CAS No.:142893-61-6
Molecular Formula:C₂₃H₃₄S₂
Molecular Weight:374.655
Hs Code.:

Synonyms:all-trans-retinal propylene dithioacetal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of all-trans-retinal propylene dithioacetal

Chemical Property:

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Technology Process of all-trans-retinal propylene dithioacetal

There total 4 articles about all-trans-retinal propylene dithioacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 142893-62-7,142927-78-4,146609-16-7
8-(1,3-dithian-2-yl)-3,7-dimethyl-1-(2,6,6-trimethyl-cyclohex-1-enyl)octa-1E,4E,7E-trien-3,6-diol

: 142893-61-6
all-trans-retinal propylene dithioacetal

Guidance literature:: With lithium aluminium tetrahydride; titanium(III) chloride; In tetrahydrofuran; for 3h; Ambient temperature;
DOI:10.1016/S0040-4039(00)92667-4

Reference yield:

: 17974-59-3
(7E)-9-ethynyl-β-ionol

: 142893-61-6
all-trans-retinal propylene dithioacetal

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) ethylmagnesium bromide / 1.) THF, r.t, 1.5 h; 2.) THF, r.t., 1 h

2: 70 percent / LiAlH₄ / tetrahydrofuran; diethyl ether / 0.5 h / 55 °C

3: 60 percent / titanium trichloride, LiAlH₄ / tetrahydrofuran; diethyl ether / 3 h / Ambient temperature

With lithium aluminium tetrahydride; titanium(III) chloride; ethylmagnesium bromide; In tetrahydrofuran; diethyl ether;

Reference yield:

: 84188-96-5
(E)-3-(1,3-dithian-2-yl)-2-methylpropenal

: 142893-61-6
all-trans-retinal propylene dithioacetal

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) ethylmagnesium bromide / 1.) THF, r.t, 1.5 h; 2.) THF, r.t., 1 h

2: 70 percent / LiAlH₄ / tetrahydrofuran; diethyl ether / 0.5 h / 55 °C

3: 60 percent / titanium trichloride, LiAlH₄ / tetrahydrofuran; diethyl ether / 3 h / Ambient temperature

With lithium aluminium tetrahydride; titanium(III) chloride; ethylmagnesium bromide; In tetrahydrofuran; diethyl ether;