(E)-2,2,2-trichloroacetimidic acid 4-phenylbut-2-enyl ester

Base Information

• Chemical Name: (E)-2,2,2-trichloroacetimidic acid 4-phenylbut-2-enyl ester
• CAS No.: 1033605-70-7
• Molecular Formula: C₁₂H₁₂Cl₃NO
• Molecular Weight: 292.592
• Mol file: 1033605-70-7.mol

Synonyms:(E)-2,2,2-trichloroacetimidic acid 4-phenylbut-2-enyl ester

Chemical Property of (E)-2,2,2-trichloroacetimidic acid 4-phenylbut-2-enyl ester

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of (E)-2,2,2-trichloroacetimidic acid 4-phenylbut-2-enyl ester

There total 1 articles about (E)-2,2,2-trichloroacetimidic acid 4-phenylbut-2-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

(2E)-4-phenylbut-2-en-1-ol (42238-15-3,22910-59-4,49676-93-9) + trichloroacetonitrile (545-06-2) → (E)-2,2,2-trichloroacetimidic acid 4-phenylbut-2-enyl ester (1033605-70-7)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 ℃; for 1h;

DOI:10.1002/chem.200700873

Reference yield:

(E)-2,2,2-trichloroacetimidic acid 4-phenylbut-2-enyl ester (1033605-70-7) → (S)-2,2,2-trichloro-N-(1-benzylallyl)acetamide (1033605-74-1) + (R)-2,2,2-trichloro-N-(1-benzylallyl)acetamide

Guidance literature:

(S)-dichloro cobalt oxazoline palladacycle; In acetonitrile; at 70 ℃; for 48h; Title compound not separated from byproducts.;

DOI:10.1002/chem.200700873

upstream raw materials:

(2E)-4-phenylbut-2-en-1-ol

trichloroacetonitrile

Downstream raw materials:

(S)-2,2,2-trichloro-N-(1-benzylallyl)acetamide