2-[(4,4-dimethyl-2,6-dioxocyclohexylidene)methyl]-1H-indol-3-yl 4-methylbenzenesulfonate

Base Information

Chemical Name:2-[(4,4-dimethyl-2,6-dioxocyclohexylidene)methyl]-1H-indol-3-yl 4-methylbenzenesulfonate
CAS No.:140836-26-6
Molecular Formula:C₂₄H₂₃NO₅S
Molecular Weight:437.516
Hs Code.:
Mol file:140836-26-6.mol

Synonyms:5,5-dimethyl-2-(3-tosyloxyindol-2-ylmethylene)cyclohexane-1,3-dione

Suppliers and Price of 2-[(4,4-dimethyl-2,6-dioxocyclohexylidene)methyl]-1H-indol-3-yl 4-methylbenzenesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-[(4,4-dimethyl-2,6-dioxocyclohexylidene)methyl]-1H-indol-3-yl 4-methylbenzenesulfonate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-[(4,4-dimethyl-2,6-dioxocyclohexylidene)methyl]-1H-indol-3-yl 4-methylbenzenesulfonate

There total 4 articles about 2-[(4,4-dimethyl-2,6-dioxocyclohexylidene)methyl]-1H-indol-3-yl 4-methylbenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 140836-18-6
5,5-dimethyl-2-(3-hydroxyindol-2-ylmethylene)cyclohexane-1,3-dione

: 98-59-9
p-toluenesulfonyl chloride

: 140836-26-6
5,5-dimethyl-2-(3-tosyloxyindol-2-ylmethylene)cyclohexane-1,3-dione

Guidance literature:: With pyridine; at 20 ℃; for 24h;
DOI:10.1007/BF00484358

Reference yield: 50.0%

: 126-81-8
dimedone

: 136203-30-0
2-formyl-3-tosyloxyindole

: 140836-26-6
5,5-dimethyl-2-(3-tosyloxyindol-2-ylmethylene)cyclohexane-1,3-dione

Guidance literature:: With triethylamine; In benzene; at 20 ℃; for 24h;
DOI:10.1007/BF00484358

Reference yield:

: 126-81-8
dimedone

: 140836-26-6
5,5-dimethyl-2-(3-tosyloxyindol-2-ylmethylene)cyclohexane-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / benzene / 3 h / Heating

2: 56 percent / pyridine / 24 h / 20 °C

With pyridine; In benzene;
DOI:10.1007/BF00484358