2-Chloro-3-iodophenyl diethylcarbamate

Base Information

Chemical Name:2-Chloro-3-iodophenyl diethylcarbamate
CAS No.:863870-84-2
Molecular Formula:C11H13 Cl I N O2
Molecular Weight:353.587
Hs Code.:
DSSTox Substance ID:DTXSID70463567
Mol file:863870-84-2.mol

Synonyms:863870-84-2;2-Chloro-3-iodophenyl diethylcarbamate;2-CHLORO-3-IODOPHENYL N,N-DIETHYLCARBAMATE;(2-chloro-3-iodophenyl) N,N-diethylcarbamate;2-CHLORO-3-IODOPHENYLN,N-DIETHYLCARBAMATE;DTXSID70463567

Suppliers and Price of 2-Chloro-3-iodophenyl diethylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-CHLORO-3-IODOPHENYL N,N-DIETHYLCARBAMATE 95.00%
5MG
$ 499.93

Total 4 raw suppliers

Chemical Property of 2-Chloro-3-iodophenyl diethylcarbamate

Chemical Property:

PSA：29.54000
LogP:3.78520
XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:352.96795
Heavy Atom Count:16
Complexity:236

Purity/Quality:

97% ^*data from raw suppliers

2-CHLORO-3-IODOPHENYL N,N-DIETHYLCARBAMATE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)C(=O)OC1=C(C(=CC=C1)I)Cl

Technology Process of 2-Chloro-3-iodophenyl diethylcarbamate

There total 3 articles about 2-Chloro-3-iodophenyl diethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 863870-73-9
O-3-iodophenyl N,N-diethylcarbamate

: 863870-84-2
O-2-chloro-3-iodophenyl N,N-diethylcarbamate

Guidance literature:: O-3-iodophenyl N,N-diethylcarbamate; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

With hexachloroethane; In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1021/jo0508402

Reference yield:

: 626-02-8
3-Iodophenol

: 863870-84-2
O-2-chloro-3-iodophenyl N,N-diethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / tetrahydrofuran / 20 °C

1.2: 95 percent / tetrahydrofuran / 8 h / 20 °C

2.1: LDA / tetrahydrofuran; hexane / 0.5 h / -78 °C

2.2: 70 percent / hexachloroethane / tetrahydrofuran; hexane / -78 - 20 °C

With sodium hydride; lithium diisopropyl amide; In tetrahydrofuran; hexane;
DOI:10.1021/jo0508402

Reference yield:

: 88-10-8
N,N-diethylcarbamyl chloride

: 863870-84-2
O-2-chloro-3-iodophenyl N,N-diethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / tetrahydrofuran / 20 °C

1.2: 95 percent / tetrahydrofuran / 8 h / 20 °C

2.1: LDA / tetrahydrofuran; hexane / 0.5 h / -78 °C

2.2: 70 percent / hexachloroethane / tetrahydrofuran; hexane / -78 - 20 °C

With sodium hydride; lithium diisopropyl amide; In tetrahydrofuran; hexane;
DOI:10.1021/jo0508402