C₄₅H₄₆F₆N₂O₉

Base Information

Chemical Name:C₄₅H₄₆F₆N₂O₉
CAS No.:1597488-31-7
Molecular Formula:C₄₅H₄₆F₆N₂O₉
Molecular Weight:872.859
Hs Code.:

C<sub>45</sub>H<sub>46</sub>F<sub>6</sub>N<sub>2</sub>O<sub>9</sub>

Synonyms:C₄₅H₄₆F₆N₂O₉

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₅H₄₆F₆N₂O₉

Chemical Property:

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Technology Process of C₄₅H₄₆F₆N₂O₉

There total 6 articles about C₄₅H₄₆F₆N₂O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: C₁₇H₂₀F₃NO₅

: 1597488-16-8
C₃₀H₃₀F₃NO₆

: 1597488-31-7
C₄₅H₄₆F₆N₂O₉

Guidance literature:: With calcium sulfate; scandium tris(trifluoromethanesulfonate); In 1,2-dichloro-ethane; at -30 - 20 ℃; for 11h;
DOI:10.1002/anie.201308016

Reference yield:

: 79383-44-1
methyl 2-methyl-6-methoxybenzoate

: 1597488-31-7
C₄₅H₄₆F₆N₂O₉

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C

1.2: 0.33 h / -78 °C

1.3: -78 - 20 °C

2.1: boron tribromide / dichloromethane / 6 h / -78 - 0 °C

3.1: trimethylsilyl trifluoromethanesulfonate; calcium sulfate / 1,2-dichloro-ethane / 3 h / -30 - -10 °C / Inert atmosphere

4.1: scandium tris(trifluoromethanesulfonate); calcium sulfate / 1,2-dichloro-ethane / 11 h / -30 - 20 °C

With calcium sulfate; trimethylsilyl trifluoromethanesulfonate; boron tribromide; scandium tris(trifluoromethanesulfonate); lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1002/anie.201308016

Reference yield:

: 79482-37-4
3,4-dihydro-9-hydroxy-8-methoxyanthracen-1(2H)-one

: 1597488-31-7
C₄₅H₄₆F₆N₂O₉

Guidance literature:: Multi-step reaction with 3 steps

1: trimethylsilyl trifluoromethanesulfonate; calcium sulfate / 1,2-dichloro-ethane / 7 h / -30 - 10 °C / Inert atmosphere

2: magnesium iodide diethyletherate / diethyl ether; tetrahydrofuran / 5 h / 0 - 50 °C

3: scandium tris(trifluoromethanesulfonate); calcium sulfate / 1,2-dichloro-ethane / 11 h / -30 - 20 °C

With calcium sulfate; magnesium iodide diethyletherate; trimethylsilyl trifluoromethanesulfonate; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; diethyl ether; 1,2-dichloro-ethane;
DOI:10.1002/anie.201308016