C₄₅H₆₂O₁₀

Base Information

• Chemical Name: C₄₅H₆₂O₁₀
• CAS No.: 161984-90-3
• Molecular Formula: C₄₅H₆₂O₁₀
• Molecular Weight: 762.981
• Mol file: 161984-90-3.mol

Synonyms:C₄₅H₆₂O₁₀

Chemical Property of C₄₅H₆₂O₁₀

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₅H₆₂O₁₀

There total 19 articles about C₄₅H₆₂O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

C51H76O10Si (161984-89-0) → C45H62O10 (161984-90-3)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 25 ℃; for 2h;

DOI:10.1021/ja00108a052 DOI:10.1021/ja00146a010

Reference yield:

C45H62O9 (161984-86-7) → C45H62O10 (161984-90-3)

Guidance literature:

Multi-step reaction with 6 steps

1: 435 mg / pyridinium p-toluenesulfonate / CH₂Cl₂ / 14 h / 0 °C

2: 2,6-lutidine / CH₂Cl₂ / 0.25 h / 0 °C

3: 1.) O₃, 2.) Ph₃P / 1.) CH₂Cl₂, -78 deg C, 2.) CH₂Cl₂, 25 deg C, 1 h

4: tetrahydrofuran / 0.5 h / 0 °C

5: Dess-Martin periodinane / CH₂Cl₂ / 2 h / 25 °C

6: 90 percent / TBAF / tetrahydrofuran / 2 h / 25 °C

With 2,6-dimethylpyridine; tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; Dess-Martin periodane; ozone; triphenylphosphine; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ja00146a010

Reference yield:

C45H62O9 (170707-12-7) → C45H62O10 (161984-90-3)

Guidance literature:

Multi-step reaction with 5 steps

1: 2,6-lutidine / CH₂Cl₂ / 0.25 h / 0 °C

2: 1.) O₃, 2.) Ph₃P / 1.) CH₂Cl₂, -78 deg C, 2.) CH₂Cl₂, 25 deg C, 1 h

3: tetrahydrofuran / 0.5 h / 0 °C

4: Dess-Martin periodinane / CH₂Cl₂ / 2 h / 25 °C

5: 90 percent / TBAF / tetrahydrofuran / 2 h / 25 °C

With 2,6-dimethylpyridine; tetrabutyl ammonium fluoride; Dess-Martin periodane; ozone; triphenylphosphine; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ja00146a010

upstream raw materials:

C₅₁H₇₆O₁₀Si

C₄₅H₆₂O₉

C₄₅H₆₂O₉

C₄₈H₇₂O₉Si

Downstream raw materials:

C₄₇H₆₃BrO₁₁

C₄₀H₅₈O₁₁S

C₄₇H₆₄O₉

C₄₇H₆₂O₁₀