(Z)-N-<(2S)-2-(tert-butyldiphenylsilyloxy)propylidene>benzylamine N-oxide

Base Information

Chemical Name:(Z)-N-<(2S)-2-(tert-butyldiphenylsilyloxy)propylidene>benzylamine N-oxide
CAS No.:162740-16-1
Molecular Formula:C₂₆H₃₁NO₂Si
Molecular Weight:417.623
Hs Code.:

Synonyms:(Z)-N-<(2S)-2-(tert-butyldiphenylsilyloxy)propylidene>benzylamine N-oxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-N-<(2S)-2-(tert-butyldiphenylsilyloxy)propylidene>benzylamine N-oxide

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Technology Process of (Z)-N-<(2S)-2-(tert-butyldiphenylsilyloxy)propylidene>benzylamine N-oxide

There total 1 articles about (Z)-N-<(2S)-2-(tert-butyldiphenylsilyloxy)propylidene>benzylamine N-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 87696-33-1
(S)-2-(O-tert-butyldiphenylsilyloxy)propanal

: 622-30-0
N-benzyl hydroxylalmine

: 162740-16-1
(Z)-N-<(2S)-2-(tert-butyldiphenylsilyloxy)propylidene>benzylamine N-oxide

Guidance literature:: With magnesium sulfate; In dichloromethane; for 4h; Ambient temperature;
DOI:10.1080/00397919408010565

Reference yield: 47.0%

: 3034-53-5,215777-74-5
2-bromo-1,3-thiazole

: 162740-16-1
(Z)-N-<(2S)-2-(tert-butyldiphenylsilyloxy)propylidene>benzylamine N-oxide

: 173522-39-9
N-Benzyl-2-O-(tert-butyldiphenylsilyl)-1,3-dideoxy-1-(hydroxyamino)-1-(2-thiazolyl)-L-erythro-triitol

: 173382-56-4
N-Benzyl-2-O-(tert-butyldiphenylsilyl)-1,3-dideoxy-1-(hydroxyamino)-1-(2-thiazolyl)-L-threo-triitol

Guidance literature:: In tetrahydrofuran; diethyl ether; hexane; Yields of byproduct given; 1.) -78 deg C, 15 min, 2.) -80 deg C, 15 min;

Reference yield:

: 162740-16-1
(Z)-N-<(2S)-2-(tert-butyldiphenylsilyloxy)propylidene>benzylamine N-oxide

: (1S,2S)-2-(tert-Butyl-diphenyl-silanyloxy)-1-thiazol-2-yl-propylamine

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether; tetrahydrofuran; hexane / 1.) -78 deg C, 15 min, 2.) -80 deg C, 15 min

2: 20percent aq. TiCl₃ / methanol / 0.25 h / Ambient temperature

With titanium(III) chloride; In tetrahydrofuran; methanol; diethyl ether; hexane;