N₁-{[2-(5-benzyl-1H-tetrazol-1-yl)-1-(4-chlorophenyl)ethoxy]acetyl}-N₄-phenylthiosemicarbazide

Base Information

• Chemical Name: N₁-{[2-(5-benzyl-1H-tetrazol-1-yl)-1-(4-chlorophenyl)ethoxy]acetyl}-N₄-phenylthiosemicarbazide
• CAS No.: 1156501-47-1
• Molecular Formula: C₂₅H₂₄ClN₇O₂S
• Molecular Weight: 522.03

Synonyms:N₁-{[2-(5-benzyl-1H-tetrazol-1-yl)-1-(4-chlorophenyl)ethoxy]acetyl}-N₄-phenylthiosemicarbazide

Chemical Property of N₁-{[2-(5-benzyl-1H-tetrazol-1-yl)-1-(4-chlorophenyl)ethoxy]acetyl}-N₄-phenylthiosemicarbazide

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Technology Process of N₁-{[2-(5-benzyl-1H-tetrazol-1-yl)-1-(4-chlorophenyl)ethoxy]acetyl}-N₄-phenylthiosemicarbazide

There total 1 articles about N₁-{[2-(5-benzyl-1H-tetrazol-1-yl)-1-(4-chlorophenyl)ethoxy]acetyl}-N₄-phenylthiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2-[2-(5-benzyl-1H-tetrazol-1-yl)-1-(4-chlorophenyl)ethoxy]acetohydrazide (1156501-39-1) + phenyl isothiocyanate (103-72-0) → N1-{[2-(5-benzyl-1H-tetrazol-1-yl)-1-(4-chlorophenyl)ethoxy]acetyl}-N4-phenylthiosemicarbazide (1156501-47-1)

Guidance literature:

In ethanol; at 20 ℃; for 3h;

DOI:10.1016/j.bmc.2009.02.004

Reference yield: 85.0%

N1-{[2-(5-benzyl-1H-tetrazol-1-yl)-1-(4-chlorophenyl)ethoxy]acetyl}-N4-phenylthiosemicarbazide (1156501-47-1) → 5-{[2-(5-benzyl-1H-tetrazol-1-yl)-1-(4-chlorophenyl)ethoxy]methyl}-4-phenyl-4H-1,2,4-triazole-3-thiol (1156501-50-6)

Guidance literature:

N₁-{[2-(5-benzyl-1H-tetrazol-1-yl)-1-(4-chlorophenyl)ethoxy]acetyl}-N₄-phenylthiosemicarbazide; With sodium carbonate; In water; for 2h; Reflux;

With hydrogenchloride; In water;

DOI:10.1016/j.bmc.2009.02.004

Reference yield: 52.0%

N1-{[2-(5-benzyl-1H-tetrazol-1-yl)-1-(4-chlorophenyl)ethoxy]acetyl}-N4-phenylthiosemicarbazide (1156501-47-1) → 2-{[2-(5-benzyl-1H-tetrazol-1-yl)-1-(4-chlorophenyl)ethoxy]methyl}-5-phenylamino-1,3,4-oxadiazole (1156501-54-0)

Guidance literature:

With mercury(II) oxide; In 1,4-dioxane; for 4h; Reflux;

DOI:10.1016/j.bmc.2009.02.004

upstream raw materials:

2-[2-(5-benzyl-1H-tetrazol-1-yl)-1-(4-chlorophenyl)ethoxy]acetohydrazide

phenyl isothiocyanate

Downstream raw materials:

5-{[2-(5-benzyl-1H-tetrazol-1-yl)-1-(4-chlorophenyl)ethoxy]methyl}-4-phenyl-4H-1,2,4-triazole-3-thiol

2-{[2-(5-benzyl-1H-tetrazol-1-yl)-1-(4-chlorophenyl)ethoxy]methyl}-5-phenylamino-1,3,4-oxadiazole

6-(4-chlorophenyl)-5,6-dihydro-11H-tetrazolo[1,5-a]benz[d]azepine

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