C₃₄H₅₃BrN₄O₇Si

Base Information

Chemical Name:C₃₄H₅₃BrN₄O₇Si
CAS No.:434308-80-2
Molecular Formula:C₃₄H₅₃BrN₄O₇Si
Molecular Weight:737.807
Hs Code.:

C<sub>34</sub>H<sub>53</sub>BrN<sub>4</sub>O<sub>7</sub>Si

Synonyms:C₃₄H₅₃BrN₄O₇Si

Suppliers and Price of C₃₄H₅₃BrN₄O₇Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₄H₅₃BrN₄O₇Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₄H₅₃BrN₄O₇Si

There total 22 articles about C₃₄H₅₃BrN₄O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 434308-56-2
(3S,4S)-5-(4-bromobenzyloxy)-4-hydroxylamino-3-methylpent-1-ene

: 434308-58-4
(3R,4S)-3-(tert-butyloxycarbonyl)amino-4-(tert-butyldimethylsilanyloxy)-4-(2,6-dimethoxypyrimidin-4-yl)butanal

: 434308-80-2
C₃₄H₅₃BrN₄O₇Si

Guidance literature:: In methanol; for 5h; Heating;
DOI:10.1021/jo0486387

Reference yield:

: 400837-92-5
2-(4-bromobenzyloxy)ethanol

: 434308-80-2
C₃₄H₅₃BrN₄O₇Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: Dess-Martin periodinane / CH₂Cl₂ / 2 h / 24 °C

2.1: n-BuLi; t-BuOK; (+)-(Ipc)2BOMe / BF₃*OEt₂ / tetrahydrofuran; hexane; diethyl ether / 5 h / -78 °C

2.2: 45 percent / aq. NaOH; H₂O₂ / tetrahydrofuran; hexane; diethyl ether / 1 h / Heating

3.1: pyridine; DMAP / CH₂Cl₂ / 16 h / 24 °C

4.1: NaN₃ / dimethylformamide / 16 h / 85 °C

5.1: 7.0 mg / PPh₃ / tetrahydrofuran; H₂O / 4 h / 55 °C

6.1: Na₂CO₃ / methanol / 17 h / 24 - 60 °C

7.1: m-CPBA / CH₂Cl₂ / 2 h / 24 °C

8.1: 25.6 mg / NH₂OH*HCl / methanol / 2 h / 0 °C

9.1: 60 percent / methanol / 5 h / Heating

With pyridine; dmap; n-butyllithium; sodium azide; hydroxylamine hydrochloride; potassium tert-butylate; sodium carbonate; Dess-Martin periodane; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; (+)-B-methoxydiisocamphenylborane; boron trifluoride diethyl etherate; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; water; N,N-dimethyl-formamide; 1.1: Dess-Martin oxidation;
DOI:10.1021/jo0486387

Reference yield:

: 60186-89-2
4-bromo-2,6-dimethoxy-pyrimidine

: 434308-80-2
C₃₄H₅₃BrN₄O₇Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: 97 percent / CeCl₃; n-BuLi / tetrahydrofuran; diethyl ether / 5.75 h / -78 - 24 °C

2.1: 93 percent / Et₃N; DMAP / CH₂Cl₂ / 5 h / Heating

3.1: 84 percent / L-Selectride / tetrahydrofuran / 1.5 h / -78 °C

4.1: 87 percent / 2,6-lutidine / CH₂Cl₂ / 1.25 h

5.1: formic acid / diethyl ether / 12 h

5.2: 100 percent / K₂CO₃ / methanol / 1 h

6.1: H₂ / Pd(OH)2/C / ethanol / 7 h

7.1: 68 percent / Et₃N / CH₂Cl₂ / 24 h / 24 °C

8.1: 91 percent / N-methylmorpholine N-oxide; tetra-n-propylammonium perruthenate / CH₂Cl₂ / 0.75 h / 24 °C

9.1: 60 percent / methanol / 5 h / Heating

With 2,6-dimethylpyridine; dmap; n-butyllithium; formic acid; cerium(III) chloride; tetrapropylammonium perruthennate; hydrogen; L-Selectride; 4-methylmorpholine N-oxide; triethylamine; palladium dihydroxide; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane;
DOI:10.1021/jo0486387