2-(4-(3-hydroxyphenyl)-6-morpholino-1,3,5-triazin-2-ylamino)-N-methylacetamide

Base Information

Chemical Name:2-(4-(3-hydroxyphenyl)-6-morpholino-1,3,5-triazin-2-ylamino)-N-methylacetamide
CAS No.:1391925-33-9
Molecular Formula:C₁₆H₂₀N₆O₃
Molecular Weight:344.373
Hs Code.:

Synonyms:2-(4-(3-hydroxyphenyl)-6-morpholino-1,3,5-triazin-2-ylamino)-N-methylacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(4-(3-hydroxyphenyl)-6-morpholino-1,3,5-triazin-2-ylamino)-N-methylacetamide

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Technology Process of 2-(4-(3-hydroxyphenyl)-6-morpholino-1,3,5-triazin-2-ylamino)-N-methylacetamide

There total 3 articles about 2-(4-(3-hydroxyphenyl)-6-morpholino-1,3,5-triazin-2-ylamino)-N-methylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: C₁₀H₁₅ClN₆O₂

: 214360-76-6
3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenol

: 1391925-33-9
2-(4-(3-hydroxyphenyl)-6-morpholino-1,3,5-triazin-2-ylamino)-N-methylacetamide

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,2-dimethoxyethane; water; at 120 ℃; for 0.333333h; Inert atmosphere; Microwave irradiation;
DOI:10.1021/acsmedchemlett.5b00322

Reference yield:

: 6601-22-5
2,6-Dichloro-4-morpholino-1,3,5-triazine

: 1391925-33-9
2-(4-(3-hydroxyphenyl)-6-morpholino-1,3,5-triazin-2-ylamino)-N-methylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / acetone; water / 16 h / 20 °C

2: sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,2-dimethoxyethane / 0.33 h / 120 °C / Inert atmosphere; Microwave irradiation

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydrogencarbonate; sodium carbonate; In 1,2-dimethoxyethane; water; acetone; 2: |Suzuki Coupling;
DOI:10.1021/acsmedchemlett.5b00322