di-(-)-(1R,2S)-2-phenyl-1-cyclohexyl diazane-1,2-dicarboxylate

Base Information

Chemical Name:di-(-)-(1R,2S)-2-phenyl-1-cyclohexyl diazane-1,2-dicarboxylate
CAS No.:206359-90-2
Molecular Formula:C₂₆H₃₂N₂O₄
Molecular Weight:436.551
Hs Code.:

Synonyms:di-(-)-(1R,2S)-2-phenyl-1-cyclohexyl diazane-1,2-dicarboxylate

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Chemical Property of di-(-)-(1R,2S)-2-phenyl-1-cyclohexyl diazane-1,2-dicarboxylate

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Technology Process of di-(-)-(1R,2S)-2-phenyl-1-cyclohexyl diazane-1,2-dicarboxylate

There total 1 articles about di-(-)-(1R,2S)-2-phenyl-1-cyclohexyl diazane-1,2-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 206359-89-9
(-)-(1R)-trans-2-phenylcyclohexyl chloroformate

: 206359-90-2
di-(-)-(1R,2S)-2-phenyl-1-cyclohexyl diazane-1,2-dicarboxylate

Guidance literature:: With quinoline; hydrazine hydrate; In tetrahydrofuran; at 0 - 20 ℃; for 24h; Yield given;
DOI:10.1016/S0957-4166(98)00034-2

Reference yield: 97.0%

: 206359-90-2
di-(-)-(1R,2S)-2-phenyl-1-cyclohexyl diazane-1,2-dicarboxylate

: 206359-91-3
di-(-)-(1R,2S)-2-phenyl-1-cyclohexyl diazene-1,2-dicarboxylate

Guidance literature:: With pyridine; N-Bromosuccinimide; In dichloromethane; at 0 - 5 ℃; for 0.25h;
DOI:10.1016/S0957-4166(98)00034-2

Reference yield:

: 206359-90-2
di-(-)-(1R,2S)-2-phenyl-1-cyclohexyl diazane-1,2-dicarboxylate

: di-(-)-(1R,2S)-2-phenylcyclohexyl 1-(2'-cyclohexen-1'-yl)-1,2-diazanedicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / N-bromosuccinimide, pyridine / CH₂Cl₂ / 0.25 h / 0 - 5 °C

2: 80 percent / SnCl₄ / CH₂Cl₂ / 0.08 h / -60 °C

With pyridine; N-Bromosuccinimide; tin(IV) chloride; In dichloromethane;
DOI:10.1016/S0957-4166(98)00034-2