C₄₁H₄₃NO₁₀S

Base Information

Chemical Name:C₄₁H₄₃NO₁₀S
CAS No.:922178-33-4
Molecular Formula:C₄₁H₄₃NO₁₀S
Molecular Weight:741.859
Hs Code.:

C<sub>41</sub>H<sub>43</sub>NO<sub>10</sub>S

Synonyms:C₄₁H₄₃NO₁₀S

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Chemical Property of C₄₁H₄₃NO₁₀S

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Technology Process of C₄₁H₄₃NO₁₀S

There total 13 articles about C₄₁H₄₃NO₁₀S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 922178-31-2
C₅₃H₇₁NO₁₀SSi₂

: 922178-33-4
C₄₁H₄₃NO₁₀S

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1139/V06-078

Reference yield:

: 130669-75-9
(3aS,7aS)-4-bromo-2,2-dimethyl-3a,7a-dihydro-1,3-benzodioxole

: 922178-33-4
C₄₁H₄₃NO₁₀S

Guidance literature:: Multi-step reaction with 9 steps

1.1: Cu(acac)2 / acetonitrile / 0 - 20 °C

2.1: n-Bu₃SnH; 2,2'-azobisisobutyronitrile / tetrahydrofuran / Heating

3.1: n-BuLi / toluene / 0.17 h / 0 °C

3.2: AlCl₃ / toluene / 18 h / 0 - 20 °C

4.1: 46 percent / N-methylmorpholine-N-oxide; OsO₄ / CH₂Cl₂ / 3 h / 20 °C

5.1: 80 percent / pyridine / 1.5 h / 20 °C

6.1: 76 percent / tetrabutylammoinum triphenyldifluorosilicate / acetonitrile / 1.5 h / 20 °C

7.1: 94 percent / sodium hexamethyldisilazide; tetrabutylammonium iodide / tetrahydrofuran / 0 - 20 °C

8.1: 31 percent / CpCo(CO)2 / xylene / 42 h / 140 °C

9.1: 72 percent / tetrabutylammonium fluoride / tetrahydrofuran / 2 h / 20 °C

With pyridine; osmium(VIII) oxide; n-butyllithium; 2,2'-azobis(isobutyronitrile); tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; sodium hexamethyldisilazane; tetra-(n-butyl)ammonium iodide; 4-methylmorpholine N-oxide; tetrabutylammonium triphenyldifluorosilicate; copper acetylacetonate; dicarbonylcyclopentadienylcobalt; In tetrahydrofuran; dichloromethane; toluene; acetonitrile; xylene;
DOI:10.1139/V06-078

Reference yield:

: 67451-62-1,82683-92-9,132958-32-8,130792-45-9
cis-(1S,2S)-1,2-dihydroxy-3-bromocyclohexa-3,5-diene

: 922178-33-4
C₄₁H₄₃NO₁₀S

Guidance literature:: Multi-step reaction with 10 steps

1.1: p-toluenesulfonic acid / acetone / 20 °C

2.1: Cu(acac)2 / acetonitrile / 0 - 20 °C

3.1: n-Bu₃SnH; 2,2'-azobisisobutyronitrile / tetrahydrofuran / Heating

4.1: n-BuLi / toluene / 0.17 h / 0 °C

4.2: AlCl₃ / toluene / 18 h / 0 - 20 °C

5.1: 46 percent / N-methylmorpholine-N-oxide; OsO₄ / CH₂Cl₂ / 3 h / 20 °C

6.1: 80 percent / pyridine / 1.5 h / 20 °C

7.1: 76 percent / tetrabutylammoinum triphenyldifluorosilicate / acetonitrile / 1.5 h / 20 °C

8.1: 94 percent / sodium hexamethyldisilazide; tetrabutylammonium iodide / tetrahydrofuran / 0 - 20 °C

9.1: 31 percent / CpCo(CO)2 / xylene / 42 h / 140 °C

10.1: 72 percent / tetrabutylammonium fluoride / tetrahydrofuran / 2 h / 20 °C

With pyridine; osmium(VIII) oxide; n-butyllithium; 2,2'-azobis(isobutyronitrile); tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; sodium hexamethyldisilazane; tetra-(n-butyl)ammonium iodide; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; tetrabutylammonium triphenyldifluorosilicate; copper acetylacetonate; dicarbonylcyclopentadienylcobalt; In tetrahydrofuran; dichloromethane; acetone; toluene; acetonitrile; xylene;
DOI:10.1139/V06-078