benzyl-6-O-allyl-3,4-O-isopropylidene-2-O-(N-imidazolylsulfonyl)-α-D-galactopyranoside

Base Information

Chemical Name:benzyl-6-O-allyl-3,4-O-isopropylidene-2-O-(N-imidazolylsulfonyl)-α-D-galactopyranoside
CAS No.:110911-41-6
Molecular Formula:C₂₂H₂₈N₂O₈S
Molecular Weight:480.539
Hs Code.:

Synonyms:benzyl-6-O-allyl-3,4-O-isopropylidene-2-O-(N-imidazolylsulfonyl)-α-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl-6-O-allyl-3,4-O-isopropylidene-2-O-(N-imidazolylsulfonyl)-α-D-galactopyranoside

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Technology Process of benzyl-6-O-allyl-3,4-O-isopropylidene-2-O-(N-imidazolylsulfonyl)-α-D-galactopyranoside

There total 1 articles about benzyl-6-O-allyl-3,4-O-isopropylidene-2-O-(N-imidazolylsulfonyl)-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53994-53-9
(3aS,4R,6S,7R,7aR)-4-Allyloxymethyl-6-benzyloxy-2,2-dimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-ol

: 7189-69-7
N,N`-sulfuryldiimidazole

: 110911-41-6
benzyl-6-O-allyl-3,4-O-isopropylidene-2-O-(N-imidazolylsulfonyl)-α-D-galactopyranoside

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1) DMF, 0 deg C then RT, 30 min 2) DMF, -40 deg C;
DOI:10.1016/S0008-6215(00)90130-7

Reference yield: 40.0%

: 110911-41-6
benzyl-6-O-allyl-3,4-O-isopropylidene-2-O-(N-imidazolylsulfonyl)-α-D-galactopyranoside

: 110911-42-7
benzyl-O-allyl-2-azido-2-desoxy-3,4-O-isopropylidene-α-D-talopyranoside

: 1-(R,S)-6-allyl-2,5-anhydro-1-C-azido-1-O-benzyl-D-talitol

Guidance literature:: With tetrabutylammoniun azide; In toluene; at 80 ℃; for 6h;
DOI:10.1016/S0008-6215(00)90130-7

Reference yield:

: 110911-41-6
benzyl-6-O-allyl-3,4-O-isopropylidene-2-O-(N-imidazolylsulfonyl)-α-D-galactopyranoside

: 110911-43-8
benzyl-2-acetamido-6-O-allyl-2-desoxy-3,4-O-isopropylidene-α-D-talopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutylammonium azide / toluene / 6 h / 80 °C

2: 1) LiAlH₄ 2) pyridine / 1) THF 2) MeOH

With pyridine; lithium aluminium tetrahydride; tetrabutylammoniun azide; In toluene;
DOI:10.1016/S0008-6215(00)90130-7