(1S,2R,5R,6S)-6-acetamido-2,3-dibromo-5-(1-ethylpropoxy)-cyclohex-3-en-1-yl acetate

Base Information

Chemical Name:(1S,2R,5R,6S)-6-acetamido-2,3-dibromo-5-(1-ethylpropoxy)-cyclohex-3-en-1-yl acetate
CAS No.:1062100-77-9
Molecular Formula:C₁₅H₂₃Br₂NO₄
Molecular Weight:441.16
Hs Code.:

Synonyms:(1S,2R,5R,6S)-6-acetamido-2,3-dibromo-5-(1-ethylpropoxy)-cyclohex-3-en-1-yl acetate

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Chemical Property of (1S,2R,5R,6S)-6-acetamido-2,3-dibromo-5-(1-ethylpropoxy)-cyclohex-3-en-1-yl acetate

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Technology Process of (1S,2R,5R,6S)-6-acetamido-2,3-dibromo-5-(1-ethylpropoxy)-cyclohex-3-en-1-yl acetate

There total 3 articles about (1S,2R,5R,6S)-6-acetamido-2,3-dibromo-5-(1-ethylpropoxy)-cyclohex-3-en-1-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1062100-76-8
N-[(1R,2R,5S,6S)-4-bromo-2-(1-ethoxypropoxy)-5,6-dihydroxycyclohex-3-en-1-yl]acetamide

: 40635-67-4
acetoxyisobutyryl bromide

: 1062100-77-9
(1S,2R,5R,6S)-6-acetamido-2,3-dibromo-5-(1-ethylpropoxy)-cyclohex-3-en-1-yl acetate

Guidance literature:: In tetrahydrofuran; at 0 - 20 ℃; for 4.16667h;
DOI:10.1002/anie.200801959

Reference yield:

: 1106677-14-8
N-[(3aR,4R,5S,7aS)-4,7-dibromo-2,2-dimethyl-3a,4,5,7a-tetrahydro-1,3-benzodioxol-5-yl]acetamide

: 1062100-77-9
(1S,2R,5R,6S)-6-acetamido-2,3-dibromo-5-(1-ethylpropoxy)-cyclohex-3-en-1-yl acetate

Guidance literature:: Multi-step reaction with 4 steps

1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -10 - 0 °C

2: boron trifluoride diethyl etherate / 6 h / -10 - 0 °C

3: hydrogenchloride / methanol; water / 6 h / 50 °C

4: tetrahydrofuran / 3.5 h / 0 - 25 °C

With hydrogenchloride; boron trifluoride diethyl etherate; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; water;
DOI:10.1021/jm3008486

Reference yield:

: 1056467-86-7
(3aS,4S,5S,7aS)-8-acetyl-7-bromo-2,2-dimethyl-3a,4,5,7a-tetrahydro-4,5-epimino-1,3-benzodioxole

: 1062100-77-9
(1S,2R,5R,6S)-6-acetamido-2,3-dibromo-5-(1-ethylpropoxy)-cyclohex-3-en-1-yl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: boron trifluoride diethyl etherate / 6 h / -10 - 0 °C

2: hydrogenchloride / methanol; water / 6 h / 50 °C

3: tetrahydrofuran / 3.5 h / 0 - 25 °C

With hydrogenchloride; boron trifluoride diethyl etherate; In tetrahydrofuran; methanol; water;
DOI:10.1021/jm3008486