5-(4-Chloro-phenyl)-3-(5-cyclohexyl-1H-imidazol-2-yl)-1-(2,4-dichloro-phenyl)-4-methyl-1H-pyrazole

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Chemical Name:5-(4-Chloro-phenyl)-3-(5-cyclohexyl-1H-imidazol-2-yl)-1-(2,4-dichloro-phenyl)-4-methyl-1H-pyrazole
CAS No.:692257-76-4
Molecular Formula:C₂₅H₂₃Cl₃N₄
Molecular Weight:485.843
Hs Code.:

Synonyms:5-(4-Chloro-phenyl)-3-(5-cyclohexyl-1H-imidazol-2-yl)-1-(2,4-dichloro-phenyl)-4-methyl-1H-pyrazole

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Chemical Property of 5-(4-Chloro-phenyl)-3-(5-cyclohexyl-1H-imidazol-2-yl)-1-(2,4-dichloro-phenyl)-4-methyl-1H-pyrazole

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Technology Process of 5-(4-Chloro-phenyl)-3-(5-cyclohexyl-1H-imidazol-2-yl)-1-(2,4-dichloro-phenyl)-4-methyl-1H-pyrazole

There total 2 articles about 5-(4-Chloro-phenyl)-3-(5-cyclohexyl-1H-imidazol-2-yl)-1-(2,4-dichloro-phenyl)-4-methyl-1H-pyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 681179-07-7
5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-4-methyl-1H-pyrazole-3-carbonitrile

: 692257-76-4
5-(4-Chloro-phenyl)-3-(5-cyclohexyl-1H-imidazol-2-yl)-1-(2,4-dichloro-phenyl)-4-methyl-1H-pyrazole

Guidance literature:: 5-(4-chlorophenyl)-1-(2,4-dichlorophenyl)-4-methyl-1H-pyrazole-3-carbonitrile; lithium hexamethyldisilazane; In tetrahydrofuran; at 0 - 100 ℃; for 6h;

With Bromomethyl cyclohexyl ketone; sodium hydrogencarbonate; In tetrahydrofuran; chloroform; water; at 20 ℃; for 72h;

Reference yield:

: 168272-78-4
5-(4-Chloro-phenyl)-1-(2,4-dichloro-phenyl)-4-methyl-1H-pyrazole-3-carboxylic acid methyl ester

: 692257-76-4
5-(4-Chloro-phenyl)-3-(5-cyclohexyl-1H-imidazol-2-yl)-1-(2,4-dichloro-phenyl)-4-methyl-1H-pyrazole

Guidance literature:: Multi-step reaction with 3 steps

1.1: formamide / 20 - 100 °C

2.1: phosphorous oxychloride / 1.5 h / 0 °C / Heating / reflux

3.1: lithium hexamethyldisilazane / tetrahydrofuran / 6 h / 0 - 100 °C

3.2: 72 h / 20 °C

With phosphorous oxychloride; lithium hexamethyldisilazane; In tetrahydrofuran; formamide;