Technology Process of C20H28O4
There total 7 articles about C20H28O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
at 20 ℃;
Inert atmosphere;
DOI:10.1021/ja2041964
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tert.-butyl lithium / tetrahydrofuran; pentane / 0.08 h / -78 °C / Inert atmosphere
1.2: 0.17 h / -78 °C / Inert atmosphere
2.1: pyridinium p-toluenesulfonate / methanol / 20 °C / Inert atmosphere
3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C / Inert atmosphere
With
tert.-butyl lithium; pyridinium p-toluenesulfonate; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; methanol; dichloromethane; pentane;
DOI:10.1021/ja2041964
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: tetramethylammonium triacetoxyborohydride / acetic acid; acetonitrile / -40 - 20 °C / Inert atmosphere
2.1: pyridinium p-toluenesulfonate / acetone / 3 h / 20 °C / Inert atmosphere
3.1: tert.-butyl lithium / tetrahydrofuran; pentane / 0.08 h / -78 °C / Inert atmosphere
3.2: 0.17 h / -78 °C / Inert atmosphere
4.1: pyridinium p-toluenesulfonate / methanol / 20 °C / Inert atmosphere
5.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C / Inert atmosphere
With
tert.-butyl lithium; pyridinium p-toluenesulfonate; 3-chloro-benzenecarboperoxoic acid; tetramethylammonium triacetoxyborohydride;
In
tetrahydrofuran; methanol; dichloromethane; acetic acid; acetone; acetonitrile; pentane;
DOI:10.1021/ja2041964
