dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-isopropyl-2-nitro-propyl] ester O-ethyl ester

Base Information

• Chemical Name: dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-isopropyl-2-nitro-propyl] ester O-ethyl ester
• CAS No.: 588706-86-9
• Molecular Formula: C₂₃H₂₉NO₅S₂
• Molecular Weight: 463.619

Synonyms:dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-isopropyl-2-nitro-propyl] ester O-ethyl ester

Chemical Property of dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-isopropyl-2-nitro-propyl] ester O-ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-isopropyl-2-nitro-propyl] ester O-ethyl ester

There total 3 articles about dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-isopropyl-2-nitro-propyl] ester O-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

potassium ethyl xanthogenate (140-89-6) + acetic acid 3-(4-benzyloxy-3-methoxy-phenyl)-1-isopropyl-2-nitro-propyl ester → dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-isopropyl-2-nitro-propyl] ester O-ethyl ester (588706-86-9)

Guidance literature:

In acetic acid; acetonitrile; at 0 - 20 ℃;

DOI:10.1021/ol035027c

Reference yield:

2-(4'-benzyloxy-3'-methoxyphenyl)-1-nitroethane (21473-46-1) → dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-isopropyl-2-nitro-propyl] ester O-ethyl ester (588706-86-9)

Guidance literature:

Multi-step reaction with 3 steps

1: Et₃N; TBAF; TBDMSCl / tetrahydrofuran / 0.5 h / 0 - 20 °C

2: DMAP / CH₂Cl₂ / 2 h / 20 °C

3: 40 percent / acetonitrile; acetic acid / 0 - 20 °C

With dmap; tetrabutyl ammonium fluoride; tert-butyldimethylsilyl chloride; triethylamine; In tetrahydrofuran; dichloromethane; acetic acid; acetonitrile; 1: Henry reaction;

DOI:10.1021/ol035027c

Reference yield:

1-(4-benzyloxy-3-methoxy-phenyl)-4-methyl-2-nitro-pentan-3-ol → dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-isopropyl-2-nitro-propyl] ester O-ethyl ester (588706-86-9)

Guidance literature:

Multi-step reaction with 2 steps

1: DMAP / CH₂Cl₂ / 2 h / 20 °C

2: 40 percent / acetonitrile; acetic acid / 0 - 20 °C

With dmap; In dichloromethane; acetic acid; acetonitrile;

DOI:10.1021/ol035027c

upstream raw materials:

potassium ethyl xanthogenate

2-(4'-benzyloxy-3'-methoxyphenyl)-1-nitroethane

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 588706-86-9 dithiocarbonic acid S-[3-(4-benzyloxy-3-methoxy-phenyl)-1-isopropyl-2-nitro-propyl] ester O-ethyl ester

Send

Send

Metric Ton KG G Pound L ML

Send

Send