1-(N-benzyloxycarbonyl-L-leucyl-L-leucyl)-2-(4-hydroxybenzyl) hydrazine

Base Information

Chemical Name:1-(N-benzyloxycarbonyl-L-leucyl-L-leucyl)-2-(4-hydroxybenzyl) hydrazine
CAS No.:150650-92-3
Molecular Formula:C₂₇H₃₈N₄O₅
Molecular Weight:498.623
Hs Code.:

Synonyms:1-(N-benzyloxycarbonyl-L-leucyl-L-leucyl)-2-(4-hydroxybenzyl) hydrazine

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Chemical Property of 1-(N-benzyloxycarbonyl-L-leucyl-L-leucyl)-2-(4-hydroxybenzyl) hydrazine

Chemical Property:

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Technology Process of 1-(N-benzyloxycarbonyl-L-leucyl-L-leucyl)-2-(4-hydroxybenzyl) hydrazine

There total 3 articles about 1-(N-benzyloxycarbonyl-L-leucyl-L-leucyl)-2-(4-hydroxybenzyl) hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3504-37-8
Cbz-L-Leu-L-Leu-OMe

: 150650-92-3
1-(N-benzyloxycarbonyl-L-leucyl-L-leucyl)-2-(4-hydroxybenzyl) hydrazine

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / hydrazine hydrate / ethanol / 24 h / Ambient temperature

2: 100 percent / acetic acid / 12 h / Ambient temperature

3: 1.) NaBH₃CN, AcOH, 2.) 2N aq. NaOH / 1.) THF, RT, overnight, 2.) MeOH, RT, 4 h

With sodium hydroxide; sodium cyanoborohydride; hydrazine hydrate; acetic acid; In ethanol; acetic acid;
DOI:10.1016/0223-5234(93)90147-7

Reference yield:

: 20777-79-1
benzyl ((S)-1-(((S)-1-hydrazineyl-4-methyl-1-oxopentan-2-yl)amino)-4-methyl-1-oxopentan-2-yl)carbamate

: 150650-92-3
1-(N-benzyloxycarbonyl-L-leucyl-L-leucyl)-2-(4-hydroxybenzyl) hydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / acetic acid / 12 h / Ambient temperature

2: 1.) NaBH₃CN, AcOH, 2.) 2N aq. NaOH / 1.) THF, RT, overnight, 2.) MeOH, RT, 4 h

With sodium hydroxide; sodium cyanoborohydride; acetic acid; In acetic acid;
DOI:10.1016/0223-5234(93)90147-7

Reference yield:

: 150650-91-2
1-(N-Z-L-leucyl-L-leucyl)-2-(4-hydroxybenzal) hydrazone

: 150650-92-3
1-(N-benzyloxycarbonyl-L-leucyl-L-leucyl)-2-(4-hydroxybenzyl) hydrazine

Guidance literature:: With sodium hydroxide; sodium cyanoborohydride; acetic acid; Yield given. Multistep reaction; 1.) THF, RT, overnight, 2.) MeOH, RT, 4 h;
DOI:10.1016/0223-5234(93)90147-7