((S)-3-Acetyl-2-oxo-oxazolidin-4-yl)-acetic acid pentafluorophenyl ester

Base Information

Chemical Name:((S)-3-Acetyl-2-oxo-oxazolidin-4-yl)-acetic acid pentafluorophenyl ester
CAS No.:760979-67-7
Molecular Formula:C₁₃H₈F₅NO₅
Molecular Weight:353.202
Hs Code.:

Synonyms:((S)-3-Acetyl-2-oxo-oxazolidin-4-yl)-acetic acid pentafluorophenyl ester

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Chemical Property of ((S)-3-Acetyl-2-oxo-oxazolidin-4-yl)-acetic acid pentafluorophenyl ester

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Technology Process of ((S)-3-Acetyl-2-oxo-oxazolidin-4-yl)-acetic acid pentafluorophenyl ester

There total 5 articles about ((S)-3-Acetyl-2-oxo-oxazolidin-4-yl)-acetic acid pentafluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 14533-84-7
pentafluorophenyl trifloroacetate

: 760979-66-6
((S)-3-Acetyl-2-oxo-oxazolidin-4-yl)-acetic acid

: 760979-67-7
((S)-3-Acetyl-2-oxo-oxazolidin-4-yl)-acetic acid pentafluorophenyl ester

Guidance literature:: With pyridine; In N,N-dimethyl-formamide; at 20 ℃; for 0.75h;
DOI:10.1039/b405856a

Reference yield:

: 4515-23-5
N-benzyloxycarbonyl-L-aspartic acid anhydride

: 760979-67-7
((S)-3-Acetyl-2-oxo-oxazolidin-4-yl)-acetic acid pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: 80 percent / NaBH₄ / tetrahydrofuran / 16 h / 20 °C

2.1: aq. Cs₂CO₃ / acetone / 3 h / Heating

2.2: 60 percent / dimethylformamide / 24 h / 20 °C

3.1: 95 percent / DIEA; DMAP / dimethylformamide / 24 h / 20 °C

4.1: 100 percent / H₂ / Pd/C / ethyl acetate / 1 h / 20 °C / 2280 Torr

5.1: 100 percent / pyridine / dimethylformamide / 0.75 h / 20 °C

With pyridine; dmap; sodium tetrahydroborate; hydrogen; caesium carbonate; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; ethyl acetate; N,N-dimethyl-formamide; acetone;
DOI:10.1039/b405856a

Reference yield:

: 540496-34-2
(S)-(2-oxo)oxazolidine-4-acetic acid benzyl ester

: 760979-67-7
((S)-3-Acetyl-2-oxo-oxazolidin-4-yl)-acetic acid pentafluorophenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / DIEA; DMAP / dimethylformamide / 24 h / 20 °C

2: 100 percent / H₂ / Pd/C / ethyl acetate / 1 h / 20 °C / 2280 Torr

3: 100 percent / pyridine / dimethylformamide / 0.75 h / 20 °C

With pyridine; dmap; hydrogen; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1039/b405856a