(Z)-3-([1,1′-biphenyl]-4-yl)-2-([1,1′-biphenyl]-4-yl(3-([1,1′-biphenyl]-4-yl)-4,5-bis(4-butylphenyl)-2H-pyrrol-2-ylidene)methyl)-4,5-bis(4-butylphenyl)-1H-pyrrole

Base Information

• Chemical Name: (Z)-3-([1,1′-biphenyl]-4-yl)-2-([1,1′-biphenyl]-4-yl(3-([1,1′-biphenyl]-4-yl)-4,5-bis(4-butylphenyl)-2H-pyrrol-2-ylidene)methyl)-4,5-bis(4-butylphenyl)-1H-pyrrole
• CAS No.: 1386995-57-8
• Molecular Formula: C₈₅H₈₀N₂
• Molecular Weight: 1129.58

Synonyms:(Z)-3-([1,1′-biphenyl]-4-yl)-2-([1,1′-biphenyl]-4-yl(3-([1,1′-biphenyl]-4-yl)-4,5-bis(4-butylphenyl)-2H-pyrrol-2-ylidene)methyl)-4,5-bis(4-butylphenyl)-1H-pyrrole

Chemical Property of (Z)-3-([1,1′-biphenyl]-4-yl)-2-([1,1′-biphenyl]-4-yl(3-([1,1′-biphenyl]-4-yl)-4,5-bis(4-butylphenyl)-2H-pyrrol-2-ylidene)methyl)-4,5-bis(4-butylphenyl)-1H-pyrrole

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Technology Process of (Z)-3-([1,1′-biphenyl]-4-yl)-2-([1,1′-biphenyl]-4-yl(3-([1,1′-biphenyl]-4-yl)-4,5-bis(4-butylphenyl)-2H-pyrrol-2-ylidene)methyl)-4,5-bis(4-butylphenyl)-1H-pyrrole

There total 1 articles about (Z)-3-([1,1′-biphenyl]-4-yl)-2-([1,1′-biphenyl]-4-yl(3-([1,1′-biphenyl]-4-yl)-4,5-bis(4-butylphenyl)-2H-pyrrol-2-ylidene)methyl)-4,5-bis(4-butylphenyl)-1H-pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3-Bis-2-propanone (15762-17-1) + 1,2-bis-(4-butylphenyl)ethane-1,2-dione → (Z)-3-([1,1′-biphenyl]-4-yl)-2-([1,1′-biphenyl]-4-yl(3-([1,1′-biphenyl]-4-yl)-4,5-bis(4-butylphenyl)-2H-pyrrol-2-ylidene)methyl)-4,5-bis(4-butylphenyl)-1H-pyrrole (1386995-57-8)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium hydroxide / ethanol / 1 h / Reflux

2: ammonium acetate; acetic acid / 20 h / 110 °C / Sealed tube

With ammonium acetate; acetic acid; potassium hydroxide; In ethanol;

DOI:10.1039/c2ob26509e

Reference yield: 92.0%

(Z)-3-([1,1′-biphenyl]-4-yl)-2-([1,1′-biphenyl]-4-yl(3-([1,1′-biphenyl]-4-yl)-4,5-bis(4-butylphenyl)-2H-pyrrol-2-ylidene)methyl)-4,5-bis(4-butylphenyl)-1H-pyrrole (1386995-57-8) → 1,9,10-tri([1,1′-biphenyl]-4-yl)-2,3,7,8-tetrakis(4-butylphenyl)-5,5-difluoro-5H-dipyrrolo[1,2-c:2′,1′-f][1,3,2]diazaborinin-4-ium-5-uide

Guidance literature:

(Z)-3-([1,1′-biphenyl]-4-yl)-2-([1,1′-biphenyl]-4-yl(3-([1,1′-biphenyl]-4-yl)-4,5-bis(4-butylphenyl)-2H-pyrrol-2-ylidene)methyl)-4,5-bis(4-butylphenyl)-1H-pyrrole; With triethylamine; In dichloromethane; for 0.25h; Inert atmosphere; Reflux;

With boron trifluoride diethyl etherate; In dichloromethane; for 2h; Inert atmosphere; Reflux;

DOI:10.1039/c2ob26509e

upstream raw materials:

1,3-Bis-2-propanone

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