C₄₇H₆₇N₃O₂

Base Information

• Chemical Name: C₄₇H₆₇N₃O₂
• CAS No.: 1268822-95-2
• Molecular Formula: C₄₇H₆₇N₃O₂
• Molecular Weight: 706.068
• Mol file: 1268822-95-2.mol

Synonyms:C₄₇H₆₇N₃O₂

Chemical Property of C₄₇H₆₇N₃O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₇H₆₇N₃O₂

There total 5 articles about C₄₇H₆₇N₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

C40H60O2 (1268822-94-1) + benzyl azide (622-79-7) → C47H67N3O2 (1268822-95-2)

Guidance literature:

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In dichloromethane; water; at 25 ℃; for 18h;

DOI:10.1071/CH10319

Reference yield:

1-dodecylbromide (143-15-7) → C47H67N3O2 (1268822-95-2)

Guidance literature:

Multi-step reaction with 6 steps

1: potassium carbonate / N,N-dimethyl-formamide / 60 °C

2: trimethylsilyl bromide / chloroform / 0 °C

3: 150 °C

4: potassium tert-butylate / tetrahydrofuran / 0 - 25 °C

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 25 °C / Inert atmosphere

6: copper(ll) sulfate pentahydrate; sodium L-ascorbate / dichloromethane; water / 18 h / 25 °C

With copper(ll) sulfate pentahydrate; trimethylsilyl bromide; potassium tert-butylate; tetrabutyl ammonium fluoride; potassium carbonate; sodium L-ascorbate; In tetrahydrofuran; dichloromethane; chloroform; water; N,N-dimethyl-formamide; 3: Arbuzov reaction;

DOI:10.1071/CH10319

Reference yield:

(3,5-bis(dodecyloxy)phenyl)methanol (199192-20-6) → C47H67N3O2 (1268822-95-2)

Guidance literature:

Multi-step reaction with 5 steps

1: trimethylsilyl bromide / chloroform / 0 °C

2: 150 °C

3: potassium tert-butylate / tetrahydrofuran / 0 - 25 °C

4: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 25 °C / Inert atmosphere

5: copper(ll) sulfate pentahydrate; sodium L-ascorbate / dichloromethane; water / 18 h / 25 °C

With copper(ll) sulfate pentahydrate; trimethylsilyl bromide; potassium tert-butylate; tetrabutyl ammonium fluoride; sodium L-ascorbate; In tetrahydrofuran; dichloromethane; chloroform; water; 2: Arbuzov reaction;

DOI:10.1071/CH10319

upstream raw materials:

C₃₅H₆₅O₅P

C₄₉H₈₀O₂Si

C₄₀H₆₀O₂

benzyl azide