C₆₄H₁₀₄O₂₈

Base Information

• Chemical Name: C₆₄H₁₀₄O₂₈
• CAS No.: 1017967-79-1
• Molecular Formula: C₆₄H₁₀₄O₂₈
• Molecular Weight: 1321.51
• Mol file: 1017967-79-1.mol

Synonyms:C₆₄H₁₀₄O₂₈

Chemical Property of C₆₄H₁₀₄O₂₈

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₄H₁₀₄O₂₈

There total 3 articles about C₆₄H₁₀₄O₂₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(2-(2-methoxyethoxy)ethoxy)ethyl p-toluenesulfonate (62921-74-8,518012-62-9,58320-73-3) → C64H104O28 (1017967-79-1)

Guidance literature:

Multi-step reaction with 4 steps

1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 12 h / 80 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 60 °C

3: thionyl chloride / dichloromethane / 3 h / 20 °C

4: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 12 h / 80 °C

With lithium aluminium tetrahydride; thionyl chloride; potassium carbonate; potassium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 1: |Williamson Ether Synthesis / 4: |Williamson Ether Synthesis;

DOI:10.1021/acs.chemmater.7b02928

Reference yield:

methyl 3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)-ethoxy)benzoate (852628-92-3) → C64H104O28 (1017967-79-1)

Guidance literature:

Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 60 °C

2: thionyl chloride / dichloromethane / 3 h / 20 °C

3: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 12 h / 80 °C

With lithium aluminium tetrahydride; thionyl chloride; potassium carbonate; potassium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 3: |Williamson Ether Synthesis;

DOI:10.1021/acs.chemmater.7b02928

Reference yield:

methyl galloate (99-24-1) → C64H104O28 (1017967-79-1)

Guidance literature:

Multi-step reaction with 4 steps

1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 12 h / 80 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 60 °C

3: thionyl chloride / dichloromethane / 3 h / 20 °C

4: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 12 h / 80 °C

With lithium aluminium tetrahydride; thionyl chloride; potassium carbonate; potassium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 1: |Williamson Ether Synthesis / 4: |Williamson Ether Synthesis;

DOI:10.1021/acs.chemmater.7b02928

upstream raw materials:

methyl galloate

2-(2-(2-methoxyethoxy)ethoxy)ethyl p-toluenesulfonate

methyl 3,4,5-tris(2-(2-(2-methoxyethoxy)ethoxy)-ethoxy)benzoate

Downstream raw materials:

C₆₃H₁₀₂O₂₈