TPA-BT₃

Base Information

Chemical Name:TPA-BT₃
CAS No.:1448509-02-1
Molecular Formula:C₄₈H₃₃NS₆
Molecular Weight:816.193
Hs Code.:

Synonyms:TPA-BT₃

Suppliers and Price of TPA-BT₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of TPA-BT₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of TPA-BT₃

There total 4 articles about TPA-BT₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 31352-46-2
2-(2-thienyl)-5-vinylthiophene

: 4181-20-8
tris(4-iodophenyl)amine

: 1448509-02-1
TPA-BT₃

Guidance literature:: With potassium phosphate; palladium diacetate; In N,N-dimethyl acetamide; at 110 ℃; for 24h; Inert atmosphere;
DOI:10.1002/cjoc.201201197

Reference yield:

: 603-34-9
N,N-diphenylaminobenzene

: 1448509-02-1
TPA-BT₃

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; potassium iodide; potassium iodate / Reflux; Inert atmosphere

2: potassium phosphate; palladium diacetate / N,N-dimethyl acetamide / 24 h / 110 °C / Inert atmosphere

With potassium iodate; potassium phosphate; palladium diacetate; acetic acid; potassium iodide; In N,N-dimethyl acetamide; 2: |Heck Reaction;
DOI:10.1002/cjoc.201201197

Reference yield:

: 492-97-7
2,2'-Bithiophene

: 1448509-02-1
TPA-BT₃

Guidance literature:: Multi-step reaction with 3 steps

1: n-butyllithium / tetrahydrofuran; hexane / 1.33 h / -80 - 20 °C

2: potassium tert-butylate / tetrahydrofuran / 5 h / Cooling with ice

3: potassium phosphate; palladium diacetate / N,N-dimethyl acetamide / 24 h / 110 °C / Inert atmosphere

With potassium phosphate; n-butyllithium; potassium tert-butylate; palladium diacetate; In tetrahydrofuran; hexane; N,N-dimethyl acetamide; 2: |Wittig Olefination / 3: |Heck Reaction;
DOI:10.1002/cjoc.201201197