1,4-Bis(pentafluorophenylethynyl)benzene

Base Information

Chemical Name:1,4-Bis(pentafluorophenylethynyl)benzene
CAS No.:258506-15-9
Molecular Formula:C₂₂H₄F₁₀
Molecular Weight:458.258
Hs Code.:

Synonyms:1,4-Bis(pentafluorophenylethynyl)benzene

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Chemical Property of 1,4-Bis(pentafluorophenylethynyl)benzene

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Technology Process of 1,4-Bis(pentafluorophenylethynyl)benzene

There total 1 articles about 1,4-Bis(pentafluorophenylethynyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 935-14-8
1,4-diethynylbenzene

: 827-15-6
1,2,3,4,5-pentafluoro-6-iodobenzene

: 258506-15-9
1,4-Bis(pentafluorophenylethynyl)benzene

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; diisopropylamine; In toluene; at 95 ℃; for 48h;
DOI:10.1021/ja0209161

Reference yield: 67.0%

: Cp2Zr(η2-Ph2PCCMes)(pyridine)

: 258506-15-9
1,4-Bis(pentafluorophenylethynyl)benzene

: Cp₂Zr[2-Ph₂P-3-Mes-4-(C₆F₅)C₄]-1,4-C₆H₄-Cp₂Zr[2-Ph₂P-3-Mes-4-(C₆F₅)C₄]

Guidance literature:: In toluene; under N2; Zr-contg. compd. (0.50 mmol) and F-contg. compd. (0.25 mmol) were dissolved in toluene; stirring at ambient temp. for 16 h; the volatile compds. were removed and the solid was washed with pentane;elem. anal.;
DOI:10.1021/om801040t

Reference yield: 44.0%

: [Cp2Zr(η2-Ph2PCCPh)]2

: 258506-15-9
1,4-Bis(pentafluorophenylethynyl)benzene

: Cp₂Zr[2-Ph₂P-3-Ph-4-(C₆F₅)C₄]-1,4-C₆H₄-Cp₂Zr[2-Ph₂P-3-Ph-4-(C₆F₅)C₄]

Guidance literature:: In toluene; under N2; Zr-contg. compd. (0.40 mmol) and F-contg. compd. (0.20 mmol) were dissolved in toluene; stirring at 50°C for 16 h; cooling to ambient temp.; the solvent was removed under vac.; the solid was washed with pentane; elem. anal.;
DOI:10.1021/om801040t