triethyl 2,2',2''-[2,4-bis(3,5-di-tert-butyl-4-hydroxybenzyl)benzene-1,3,5-triyltris(oxy)]tris(acetohydrazide)

Base Information

• Chemical Name: triethyl 2,2',2''-[2,4-bis(3,5-di-tert-butyl-4-hydroxybenzyl)benzene-1,3,5-triyltris(oxy)]tris(acetohydrazide)
• CAS No.: 1619938-75-8
• Molecular Formula: C₄₂H₆₂N₆O₈
• Molecular Weight: 778.99

Synonyms:triethyl 2,2',2''-[2,4-bis(3,5-di-tert-butyl-4-hydroxybenzyl)benzene-1,3,5-triyltris(oxy)]tris(acetohydrazide)

Chemical Property of triethyl 2,2',2''-[2,4-bis(3,5-di-tert-butyl-4-hydroxybenzyl)benzene-1,3,5-triyltris(oxy)]tris(acetohydrazide)

Chemical Property:

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Technology Process of triethyl 2,2',2''-[2,4-bis(3,5-di-tert-butyl-4-hydroxybenzyl)benzene-1,3,5-triyltris(oxy)]tris(acetohydrazide)

There total 1 articles about triethyl 2,2',2''-[2,4-bis(3,5-di-tert-butyl-4-hydroxybenzyl)benzene-1,3,5-triyltris(oxy)]tris(acetohydrazide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

triethyl 2,2',2''-[2,4-bis(3,5-di-tert-butyl-4-hydroxybenzyl)benzene-1,3,5-triyltris(oxy)]triacetate (1619938-73-6) → triethyl 2,2',2''-[2,4-bis(3,5-di-tert-butyl-4-hydroxybenzyl)benzene-1,3,5-triyltris(oxy)]tris(acetohydrazide) (1619938-75-8)

Guidance literature:

With hydrazine hydrate; In water; N,N-dimethyl-formamide; for 2h; Reflux;

DOI:10.1134/S1070428014060086

Reference yield: 87.0%

triethyl 2,2',2''-[2,4-bis(3,5-di-tert-butyl-4-hydroxybenzyl)benzene-1,3,5-triyltris(oxy)]tris(acetohydrazide) (1619938-75-8) + 3,5-di-t-butyl-4-hydroxybenzaldehyde (1620-98-0) → triethyl 2,2',2''-[2,4-bis(3,5-di-tert-butyl-4-hydroxybenzyl)benzene-1,3,5-triyltris(oxy)]tris[N'-(3,5-di-tertbutyl-4-hydroxybenzylidene)acetohydrazide] (1619938-77-0)

Guidance literature:

With acetic acid; In ethanol; N,N-dimethyl-formamide; at 80 ℃; for 20h;

DOI:10.1134/S1070428014060086

Reference yield: 84.0%

3,5-di-tert-butyl-2-hydroxybenzaldehyde (37942-07-7) + triethyl 2,2',2''-[2,4-bis(3,5-di-tert-butyl-4-hydroxybenzyl)benzene-1,3,5-triyltris(oxy)]tris(acetohydrazide) (1619938-75-8) → triethyl 2,2',2''-[2,4-bis(3,5-di-tert-butyl-4-hydroxybenzyl)benzene-1,3,5-triyltris(oxy)]tris[N'-(3,5-di-tertbutyl-2-hydroxybenzylidene)acetohydrazide] (1619938-78-1)

Guidance literature:

With acetic acid; In ethanol; N,N-dimethyl-formamide; at 80 ℃; for 24h;

DOI:10.1134/S1070428014060086

upstream raw materials:

triethyl 2,2',2''-[2,4-bis(3,5-di-tert-butyl-4-hydroxybenzyl)benzene-1,3,5-triyltris(oxy)]triacetate

Downstream raw materials:

triethyl 2,2',2''-[2,4-bis(3,5-di-tert-butyl-4-hydroxybenzyl)benzene-1,3,5-triyltris(oxy)]tris[N'-(3,5-di-tertbutyl-4-hydroxybenzylidene)acetohydrazide]

triethyl 2,2',2''-[2,4-bis(3,5-di-tert-butyl-4-hydroxybenzyl)benzene-1,3,5-triyltris(oxy)]tris[N'-(3,5-di-tertbutyl-2-hydroxybenzylidene)acetohydrazide]

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