(1Z)-1-(Phenylsulfonyl)-1-penten-3-ol

Base Information

Chemical Name:(1Z)-1-(Phenylsulfonyl)-1-penten-3-ol
CAS No.:141195-85-9
Molecular Formula:C₁₁H₁₄O₃S
Molecular Weight:226.296
Hs Code.:
DSSTox Substance ID:DTXSID901288228
Nikkaji Number:J479.592J

Synonyms:DTXSID901288228;141195-85-9;(1Z)-1-(Phenylsulfonyl)-1-penten-3-ol

Suppliers and Price of (1Z)-1-(Phenylsulfonyl)-1-penten-3-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of (1Z)-1-(Phenylsulfonyl)-1-penten-3-ol

Chemical Property:

XLogP3:1.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:226.06636548
Heavy Atom Count:15
Complexity:294

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCC(C=CS(=O)(=O)C1=CC=CC=C1)O
Isomeric SMILES:CCC(/C=C\S(=O)(=O)C1=CC=CC=C1)O

Technology Process of (1Z)-1-(Phenylsulfonyl)-1-penten-3-ol

There total 4 articles about (1Z)-1-(Phenylsulfonyl)-1-penten-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 108644-06-0
(Z)-1-Benzenesulfonyl-pent-1-en-3-one

: 141195-85-9
(+/-)-(Z)-1-(phenylsulfonyl)-1-penten-3-ol

Guidance literature:: With sodium tetrahydroborate; In methanol; for 4h; Ambient temperature;
DOI:10.1021/jo00040a028

Reference yield:

: 129083-18-7
(+/-)-(phenylsulfonyl)(p-tolylsulfinyl)methane

: 141195-85-9
(+/-)-(Z)-1-(phenylsulfonyl)-1-penten-3-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / piperidine / acetonitrile / 3.5 h / 0 °C

2: 80 percent / PCC-silica gel / CH₂Cl₂ / 2 h / -18 °C / ultrasound

3: CHCl₃ / 96 h / Irradiation

4: 85 percent / sodium borohydride / methanol / 4 h / Ambient temperature

With piperidine; sodium tetrahydroborate; pyridinium chlorochromate on silica gel; In methanol; dichloromethane; chloroform; acetonitrile;
DOI:10.1021/jo00040a028

Reference yield:

: 137653-98-6
(+/-)-(E)-1-(phenylsulfonyl)-1-penten-3-ol

: 141195-85-9
(+/-)-(Z)-1-(phenylsulfonyl)-1-penten-3-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / PCC-silica gel / CH₂Cl₂ / 2 h / -18 °C / ultrasound

2: CHCl₃ / 96 h / Irradiation

3: 85 percent / sodium borohydride / methanol / 4 h / Ambient temperature

With sodium tetrahydroborate; pyridinium chlorochromate on silica gel; In methanol; dichloromethane; chloroform;
DOI:10.1021/jo00040a028