8-azido-3,5-O-benzylidene-6,7-8-trideoxy-1,2-O-isopropylidene-α-D-gluco-octose

Base Information

Chemical Name:8-azido-3,5-O-benzylidene-6,7-8-trideoxy-1,2-O-isopropylidene-α-D-gluco-octose
CAS No.:115438-67-0
Molecular Formula:C₁₈H₂₃N₃O₅
Molecular Weight:361.398
Hs Code.:

Synonyms:8-azido-3,5-O-benzylidene-6,7-8-trideoxy-1,2-O-isopropylidene-α-D-gluco-octose

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Chemical Property of 8-azido-3,5-O-benzylidene-6,7-8-trideoxy-1,2-O-isopropylidene-α-D-gluco-octose

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Technology Process of 8-azido-3,5-O-benzylidene-6,7-8-trideoxy-1,2-O-isopropylidene-α-D-gluco-octose

There total 6 articles about 8-azido-3,5-O-benzylidene-6,7-8-trideoxy-1,2-O-isopropylidene-α-D-gluco-octose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54944-49-9
(3aR,3bS,7S,7aS,8aR)-2,2-Dimethyl-5-phenyl-tetrahydro-[1,3]dioxolo[4,5]furo[3,2-d][1,3]dioxine-7-carbaldehyde

: 115438-67-0
8-azido-3,5-O-benzylidene-6,7-8-trideoxy-1,2-O-isopropylidene-α-D-gluco-octose

Guidance literature:: Multi-step reaction with 5 steps

1: CH₂Cl₂

2: 96 percent / H₂ / 1percent Pd on charcoal / ethanol

3: 93 percent / lithium aluminium hydride / diethyl ether

4: triethylamine / CH₂Cl₂ / 0 °C

5: NaN₃ / dimethylformamide

With lithium aluminium tetrahydride; sodium azide; hydrogen; triethylamine; palladium on activated charcoal; In diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)96575-4

Reference yield:

: 22164-09-6
3,5-O-benzylidene-1,2-O-isopropylidene-α-D-glucofuranoside

: 115438-67-0
8-azido-3,5-O-benzylidene-6,7-8-trideoxy-1,2-O-isopropylidene-α-D-gluco-octose

Guidance literature:: Multi-step reaction with 6 steps

1: pyridinium chlorochromate, molecular sieves / CH₂Cl₂

2: CH₂Cl₂

3: 96 percent / H₂ / 1percent Pd on charcoal / ethanol

4: 93 percent / lithium aluminium hydride / diethyl ether

5: triethylamine / CH₂Cl₂ / 0 °C

6: NaN₃ / dimethylformamide

With lithium aluminium tetrahydride; sodium azide; molecular sieve; hydrogen; triethylamine; pyridinium chlorochromate; palladium on activated charcoal; In diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)96575-4

Reference yield:

: 115438-63-6
(E)-3-((3aR,3bS,7R,7aR,8aR)-2,2-Dimethyl-5-phenyl-tetrahydro-[1,3]dioxolo[4,5]furo[3,2-d][1,3]dioxin-7-yl)-acrylic acid ethyl ester

: 115438-67-0
8-azido-3,5-O-benzylidene-6,7-8-trideoxy-1,2-O-isopropylidene-α-D-gluco-octose

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / H₂ / 1percent Pd on charcoal / ethanol

2: 93 percent / lithium aluminium hydride / diethyl ether

3: triethylamine / CH₂Cl₂ / 0 °C

4: NaN₃ / dimethylformamide

With lithium aluminium tetrahydride; sodium azide; hydrogen; triethylamine; palladium on activated charcoal; In diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)96575-4