(2S,4S)-4-[(E)-2-(4-Chloro-phenyl)-vinyl]-2-methyl-tricyclo[10.2.2.2^5,8]octadeca-1⁽¹⁵⁾,5⁽¹⁸⁾,6,8⁽¹⁷⁾,12⁽¹⁶⁾,13-hexaene

Base Information

• Chemical Name: (2S,4S)-4-[(E)-2-(4-Chloro-phenyl)-vinyl]-2-methyl-tricyclo[10.2.2.2^5,8]octadeca-1⁽¹⁵⁾,5⁽¹⁸⁾,6,8⁽¹⁷⁾,12⁽¹⁶⁾,13-hexaene
• CAS No.: 85781-47-1
• Molecular Formula: C₂₇H₂₇Cl
• Molecular Weight: 386.964

Synonyms:(2S,4S)-4-[(E)-2-(4-Chloro-phenyl)-vinyl]-2-methyl-tricyclo[10.2.2.2^5,8]octadeca-1⁽¹⁵⁾,5⁽¹⁸⁾,6,8⁽¹⁷⁾,12⁽¹⁶⁾,13-hexaene

Chemical Property of (2S,4S)-4-[(E)-2-(4-Chloro-phenyl)-vinyl]-2-methyl-tricyclo[10.2.2.2^5,8]octadeca-1⁽¹⁵⁾,5⁽¹⁸⁾,6,8⁽¹⁷⁾,12⁽¹⁶⁾,13-hexaene

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Technology Process of (2S,4S)-4-[(E)-2-(4-Chloro-phenyl)-vinyl]-2-methyl-tricyclo[10.2.2.2^5,8]octadeca-1⁽¹⁵⁾,5⁽¹⁸⁾,6,8⁽¹⁷⁾,12⁽¹⁶⁾,13-hexaene

There total 1 articles about (2S,4S)-4-[(E)-2-(4-Chloro-phenyl)-vinyl]-2-methyl-tricyclo[10.2.2.2^5,8]octadeca-1⁽¹⁵⁾,5⁽¹⁸⁾,6,8⁽¹⁷⁾,12⁽¹⁶⁾,13-hexaene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-vinylbenzyl chloride (1073-67-2,24991-47-7) + 1,3-bis-(p-vinylphenyl)propane (58845-03-7) → (2S,4S)-4-[(E)-2-(4-Chloro-phenyl)-vinyl]-2-methyl-tricyclo[10.2.2.25,8]octadeca-1(15),5(18),6,8(17),12(16),13-hexaene (85781-47-1) + (2R,4S)-4-[(E)-2-(4-Chloro-phenyl)-vinyl]-2-methyl-tricyclo[10.2.2.25,8]octadeca-1(15),5(18),6,8(17),12(16),13-hexaene (85848-74-4)

Guidance literature:

With trifluorormethanesulfonic acid; In benzene; at 50 ℃; for 0.5h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.1021/ja00352a039

upstream raw materials:

4-vinylbenzyl chloride

1,3-bis-(p-vinylphenyl)propane

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