rac-1-Glycerol-3-<(2,4-dioxo-5,5-diphenyl-3-imidazolidinyl)methoxycarbonyl>propionic acid ester

Base Information

Chemical Name:rac-1-Glycerol-3-<(2,4-dioxo-5,5-diphenyl-3-imidazolidinyl)methoxycarbonyl>propionic acid ester
CAS No.:151227-87-1
Molecular Formula:C₂₃H₂₄N₂O₈
Molecular Weight:456.452
Hs Code.:

Synonyms:rac-1-Glycerol-3-<(2,4-dioxo-5,5-diphenyl-3-imidazolidinyl)methoxycarbonyl>propionic acid ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of rac-1-Glycerol-3-<(2,4-dioxo-5,5-diphenyl-3-imidazolidinyl)methoxycarbonyl>propionic acid ester

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Technology Process of rac-1-Glycerol-3-<(2,4-dioxo-5,5-diphenyl-3-imidazolidinyl)methoxycarbonyl>propionic acid ester

There total 2 articles about rac-1-Glycerol-3-<(2,4-dioxo-5,5-diphenyl-3-imidazolidinyl)methoxycarbonyl>propionic acid ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 150994-96-0
rac-1-(2,3-O-Isopropylidene glycerol)-3-<(2,4-dioxo-5,5-diphenyl-3-imidazolidinyl)methoxycarbonyl>propionic acid ester

: 151227-87-1
rac-1-Glycerol-3-<(2,4-dioxo-5,5-diphenyl-3-imidazolidinyl)methoxycarbonyl>propionic acid ester

Guidance literature:: With triethyl borate; boric acid; In 1,4-dioxane; 1) 20 min, 100 deg C, 2) 15 min, 100 deg C, vacuum;
DOI:10.1002/ardp.19933260810

Reference yield:

: 146644-72-6
rac-1-(2,3-O-Isopropylidene glycerol)succinic acid mono ester

: 151227-87-1
rac-1-Glycerol-3-<(2,4-dioxo-5,5-diphenyl-3-imidazolidinyl)methoxycarbonyl>propionic acid ester

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / Et₃N, bis(2-oxo-3-oxazolidinyl)phosphinic acid chloride / 1 h / Ambient temperature

2: 83 percent / (EtO)3B, H₃BO₃ / dioxane / 1) 20 min, 100 deg C, 2) 15 min, 100 deg C, vacuum

With triethyl borate; boric acid; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; triethylamine; In 1,4-dioxane;
DOI:10.1002/ardp.19933260810