Technology Process of C30H28O7
There total 1 articles about C30H28O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 5 steps
1.1: 3-chloro-benzenecarboperoxoic acid / chloroform / -20 - 0 °C
2.1: aluminum isopropoxide / toluene / 5 h / 140 °C / Sealed tube
3.1: lithium diisopropyl amide / tetrahydrofuran / 0.83 h / -78 °C / Inert atmosphere
3.2: 3 h / -78 - -30 °C / Inert atmosphere
3.3: 0 - 20 °C
4.1: Dess-Martin periodane / dichloromethane / 0.5 h / 0 °C
5.1: benzeneseleninic anhydride; sodium hydrogencarbonate / chlorobenzene / 0.5 h / 70 °C
5.2: 255 / 24 h / 25 °C
With
benzeneseleninic anhydride; aluminum isopropoxide; sodium hydrogencarbonate; Dess-Martin periodane; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide;
In
tetrahydrofuran; dichloromethane; chloroform; chlorobenzene; toluene;
DOI:10.1002/chem.201204292