C₁₅H₁₉NO₇

Base Information

• Chemical Name: C₁₅H₁₉NO₇
• CAS No.: 881833-53-0
• Molecular Formula: C₁₅H₁₉NO₇
• Molecular Weight: 325.318
• Mol file: 881833-53-0.mol

Synonyms:C₁₅H₁₉NO₇

Chemical Property of C₁₅H₁₉NO₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₅H₁₉NO₇

There total 6 articles about C₁₅H₁₉NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C24H28O2Si (881833-43-8) → C15H19NO7 (881833-53-0)

Guidance literature:

Multi-step reaction with 5 steps

1: 100 percent / NBS / acetonitrile / 25 °C

2: 91 percent / t-BuLi / tetrahydrofuran / -78 °C

3: 100 percent / TBAF; H₂O / tetrahydrofuran / 25 °C

4: 98 percent / Et₃N; DMAP / CH₂Cl₂ / 25 °C

5: 77 percent / HNO₃; HOAc / 25 °C

With dmap; N-Bromosuccinimide; tetrabutyl ammonium fluoride; water; tert.-butyl lithium; nitric acid; acetic acid; triethylamine; In tetrahydrofuran; dichloromethane; acetonitrile;

DOI:10.1039/b515674b

Reference yield:

C24H27BrO2Si (881833-51-8) → C15H19NO7 (881833-53-0)

Guidance literature:

Multi-step reaction with 4 steps

1: 91 percent / t-BuLi / tetrahydrofuran / -78 °C

2: 100 percent / TBAF; H₂O / tetrahydrofuran / 25 °C

3: 98 percent / Et₃N; DMAP / CH₂Cl₂ / 25 °C

4: 77 percent / HNO₃; HOAc / 25 °C

With dmap; tetrabutyl ammonium fluoride; water; tert.-butyl lithium; nitric acid; acetic acid; triethylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1039/b515674b

Reference yield:

C27H34O3Si (881833-44-9) → C15H19NO7 (881833-53-0)

Guidance literature:

Multi-step reaction with 3 steps

1: 100 percent / TBAF; H₂O / tetrahydrofuran / 25 °C

2: 98 percent / Et₃N; DMAP / CH₂Cl₂ / 25 °C

3: 77 percent / HNO₃; HOAc / 25 °C

With dmap; tetrabutyl ammonium fluoride; water; nitric acid; acetic acid; triethylamine; In tetrahydrofuran; dichloromethane;

DOI:10.1039/b515674b

upstream raw materials:

C₂₄H₂₈O₂Si

C₂₄H₂₇BrO₂Si

C₂₇H₃₄O₃Si

C₁₁H₁₆O₃

Downstream raw materials:

(R)-(-)-neocarazostatin B

NH₂C₆HCH₃(OOCCH₃)OCH₃CH₂C(H)CH₃OOCCH₃

Refernces